2,6-二叔丁基-4-溴甲基苯酚合成路线 （共 25 条）
反应条件
bromine in tetrachloromethane
T=85°C; 4 - 5 h;
参考文献
COUNCIL OF SCIENTIFIC AND INDUSTRIAL RESEARCH
Patent: US2004/192969 A1, 2004 ;
Location in patent: Page 4 ;
反应条件
phosphorus tribromide in dichloromethane
参考文献
Kang, Tae-Souk; Jo, Hyang-Ok; Park, Woo-Kyu; Kim, Jong-Pyung; Konishi, Yasuo; Kong, Jae-Yang; Park, No-Sang; Jung, Young-Sik
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 5 p. 1663 - 1667
反应条件
2,2'-azo-bisisobutyronitrile in chloroform
19 h; Heating / reflux;
参考文献
ZIKO LTD.
Patent: WO2005/115973 A1, 2005 ;
Location in patent: Page/Page column 8-9 ;
参考文献
Monash University
Patent: US6232314 B1, 2001 ;
反应条件
acetyl-bromide in hexane
参考文献
Gorbunov, D. B.; Ershov, V. V.; Nikiforov, G. A.
Russian Chemical Bulletin, 1993 , vol. 42, # 3 p. 481 - 485
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 3 p. 526 - 529
参考文献
Cook et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 1783
参考文献
Gorbunov, D. B.; Ershov, V. V.; Nikiforov, G. A.
Russian Chemical Bulletin, 1993 , vol. 42, # 3 p. 481 - 485
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 3 p. 526 - 529
反应条件
T=59.5°C; Rate constant;
参考文献
Cook et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 1783
反应条件
1: Et3N / pentane / 6 °C / few minutes
2: 59 percent / pentane / 30 °C
View Scheme
参考文献
Omura, Kanji
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 306 - 312
反应条件
1: 85 percent / dimethylsulfoxide / 4 h / 25 °C
2: 44 percent / 0,1 M NaClO4 / anodic oxidation
View Scheme
参考文献
Rieker,A.; Kessler,H.
Tetrahedron, 1968 , vol. 24, p. 5133 - 5144
