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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-苯甲酰基苯甲醛
合成路线
（共 43 条）
20912-50-9
4-苯甲酰基苯甲醛
+
107-21-1
乙二醇
→
反应条件
103741-08-8
[4-(1,3-二氧戊环-2-基)苯基](苯基)甲酮
反应条件
aluminum oxide in tetrachloromethane 24 h; Heating;
参考文献
Kamitori, Yasuhiro; Hojo, Masaru; Masuda, Ryoichi; Yoshida, Tatsushi
Tetrahedron Letters, 1985 , vol. 26, # 39 p. 4767 - 4770
1052721-18-2
→
反应条件
20912-50-9
4-苯甲酰基苯甲醛
反应条件
1: With trimethylsilyl trifluoromethanesulfonate; diethylphosphinoethane in dichloromethane; toluene T=20°C; 1 h; 2: With diisobutylaluminium hydride in hexane; dichloromethane T=-78°C; regioselective reaction;
参考文献
Yahata, Kenzo; Minami, Masaki; Yoshikawa, Yuki; Watanabe, Kei; Fujioka, Hiromichi
Chemical and Pharmaceutical Bulletin, 2013 , vol. 61, # 12 p. 1298 - 1307
41418-67-1
→
反应条件
20912-50-9
4-苯甲酰基苯甲醛
反应条件
perchloric acid; water in dichloromethane T=0 - 20°C; 2 h;
参考文献
Ameriks, Michael K.; Arienti, Kristen L.; Axe, Frank U.; Breitenbucher, J. Guy
Patent: US2004/214857 A1, 2004 ;
Location in patent: Page 20 ;
52010-95-4
→
反应条件
20912-50-9
4-苯甲酰基苯甲醛
反应条件
dipyridinium dichromate in dichloromethane 3 h;
参考文献
Shiue, Jiann-Shyng; Lin, Mei-Huey; Fang, Jim-Min
Journal of Organic Chemistry, 1997 , vol. 62, # 14 p. 4643 - 4649
87199-17-5
4-甲酰基苯硼酸
+
98-88-4
苯甲酰氯
→
反应条件
20912-50-9
4-苯甲酰基苯甲醛
反应条件
[Pd(.eta.(5)-C5H5)Fe(.eta.(5)-C5H3-C(CH3)=N-C6H4-4-CH3)Cl(P(C6H5)3)]; potassium carbonate in toluene T=60°C; 12 h; Inert atmosphere;
参考文献
Yu, Ajuan; Shen, Lei; Cui, Xiuling; Peng, Dongpo; Wu, Yangjie
Tetrahedron, 2012 , vol. 68, # 10 p. 2283 - 2288
→
反应条件
20912-50-9
4-苯甲酰基苯甲醛
反应条件
1: C10H11NO3 With trimethylsilyl trifluoromethanesulfonate; triphenylphosphine in dichloromethane T=20°C; 1 h; 2: phenyl-magnesium bromide in dichloromethane T=0°C; regioselective reaction;
参考文献
Yahata, Kenzo; Minami, Masaki; Yoshikawa, Yuki; Watanabe, Kei; Fujioka, Hiromichi
Chemical and Pharmaceutical Bulletin, 2013 , vol. 61, # 12 p. 1298 - 1307
100-58-3
溴化苯基镁
+
105-07-7
4-氰基苯甲醛
→
反应条件
20912-50-9
4-苯甲酰基苯甲醛
反应条件
1: [4-cyanophenyl]methanone With trimethylsilyl trifluoromethanesulfonate; triphenylphosphine in dichloromethane T=20°C; 1 h; 2: phenyl-magnesium bromide With diisobutylaluminium hydride in tetrahydrofuran; dichloromethane T=20°C; 3 h; regioselective reaction;
参考文献
Yahata, Kenzo; Minami, Masaki; Yoshikawa, Yuki; Watanabe, Kei; Fujioka, Hiromichi
Chemical and Pharmaceutical Bulletin, 2013 , vol. 61, # 12 p. 1298 - 1307
88682-29-5
→
反应条件
81449-01-6
+
20912-50-9
4-苯甲酰基苯甲醛
+
52010-95-4
反应条件
N-chloro-succinimide; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate in dichloromethane 3 h; Ambient temperaturepH 8.6;
参考文献
Einhorn, Jacques; Einhorn, Cathy; Ratajczak, Fabien; Pierre, Jean-Louis
Journal of Organic Chemistry, 1996 , vol. 61, # 21 p. 7452 - 7454
87199-17-5
4-甲酰基苯硼酸
+
65-85-0
苯甲酸
→
反应条件
20912-50-9
4-苯甲酰基苯甲醛
反应条件
tris(4-methoxyphenyl)-phosphine; water; dicarbonic acid,dimethyl ester; palladium diacetate in tetrahydrofuran T=50°C; 16 h;
参考文献
Goossen, Lukas J.; Winkel, Lars; Doehring, Arno; Ghosh, Keya; Paetzold, Jens
Synlett, 2002 , # 8 p. 1237 - 1240
87199-17-5
4-甲酰基苯硼酸
+
93-97-0
苯甲酸酐
→
反应条件
20912-50-9
4-苯甲酰基苯甲醛
反应条件
[Pd(.eta.(5)-C5H5)Fe(.eta.(5)-C5H3-C(CH3)=N-C6H4-4-CH3)Cl(P(C6H5)3)]; potassium carbonate in 1,4-dioxane T=110°C; 12 h; Inert atmosphere;
参考文献
Yu, Ajuan; Shen, Lei; Cui, Xiuling; Peng, Dongpo; Wu, Yangjie
Tetrahedron, 2012 , vol. 68, # 10 p. 2283 - 2288
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