1-氯-4-(4-甲氧基苯基)硫基-苯合成路线 (共 12 条)
反应条件
caesium carbonate; 2-(diphenylphosphinyl)-benzaldoxime; copper(l) iodide in N,N-dimethyl-formamide T=90°C; 24 h;
参考文献
Zhu, Di; Xu, Lei; Wu, Fan; Wan, Boshun
Tetrahedron Letters, 2006 , vol. 47, # 32 p. 5781 - 5784
反应条件
1-(2,6-diisopropylphenyl)-3-[2-(mesitylamino)-2-oxoethyl]-1H-imidazol-3-ium bromide; palladium diacetate; sodium hexamethyldisilazane in dimethyl sulfoxide T=80°C; 12 h;
参考文献
Byeun, Aleum; Baek, Kyungkyu; Han, Min Su; Lee, Sunwoo
Tetrahedron Letters, 2013 , vol. 54, # 49 p. 6712 - 6715
反应条件
tetra(n-butyl)ammonium hydroxide in water T=50°C; 24 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Xu, Hua-Jian; Liang, Yu-Feng; Zhou, Xin-Feng; Feng, Yi-Si
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 13 p. 2562 - 2568
反应条件
1: p-chlorobenzenethiol With sodium in diethyl ether Heating; 2: 5-(p-anisyl)thianthrenium bromide in acetonitrile T=20°C;
参考文献
Qian, Ding-Quan; Liu, Bo; Shine, Henry J.; Guzman-Jimenez, Ilse Y.; Whitmire, Kenton H.
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 3 p. 139 - 147
反应条件
KOH adsorbed on neutral alumina in neat (no solvent) 0.25 h; Milling; Reagent/catalystTime;
参考文献
Mukherjee, Nirmalya; Chatterjee, Tanmay; Ranu, Brindaban C.
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 11110 - 11114
反应条件
antimony(V) pentachloride in dichloromethane T=25°C; 2 h;
参考文献
Takeuchi, Hiroshi; Hiyama, Takehiro; Kamai, Noriyoshi; Oya, Hiromi
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 11 p. 2301 - 2305
反应条件
iron; potassium carbonate in dimethyl sulfoxide; N,N-dimethyl-formamide T=120°C; 18 h; Inert atmosphere;
参考文献
Li, Yaming; Nie, Caiping; Wang, Huifeng; Li, Xiaoying; Verpoort, Francis; Duan, Chunying
European Journal of Organic Chemistry, 2011 , # 36 p. 7331 - 7338
反应条件
1: copper(l) iodide; Na2S*9H2O; sulfur / N,N-dimethyl-formamide / 15 h / 80 °C / Inert atmosphere 2: iron; potassium carbonate / dimethyl sulfoxide; N,N-dimethyl-formamide / 18 h / 120 °C / Inert atmosphere View Scheme
参考文献
Li, Yaming; Nie, Caiping; Wang, Huifeng; Li, Xiaoying; Verpoort, Francis; Duan, Chunying
European Journal of Organic Chemistry, 2011 , # 36 p. 7331 - 7338
反应条件
1.1: 69 percent / benzene / Heating 2.1: Na / diethyl ether / Heating 2.2: 1.6 percent / acetonitrile / 20 °C View Scheme
参考文献
Qian, Ding-Quan; Liu, Bo; Shine, Henry J.; Guzman-Jimenez, Ilse Y.; Whitmire, Kenton H.
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 3 p. 139 - 147
反应条件
1.) -40 deg C, 15 min, 2.) ca.20 deg C, 2 h;
参考文献
Ibragimov, M. A.; Smit, V. A.; Gybin, A. S.; Krimer, M. Z.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 1 p. 137 - 141
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 1 p. 161 - 165