in water byproducts: ammonia; Ba(OH)2*8H2O added to distd. water, soln. of NH4SCN in distd. water added, refluxed; solvent evapd., recrystd. from EtOH;
参考文献
Touaj, Khlifa; Chabanel, Martial
Journal of the Chemical Society, Faraday Transactions, 1995 , vol. 91, # 24 p. 4395 - 4402
in neat (no solvent) metal-salt:NaSCN molar ratio was 1:1, 340 °C in a silica-ampoule,reaction may be proceed at 150 °C with eutectics of NaSCN:KSCN ( 7:3); cooling rate was 1 °/h;
参考文献
Wickleder, Claudia
Zeitschrift fur Anorganische und Allgemeine Chemie, 2001 , vol. 627, # 7 p. 1693 - 1698
Tscherniac
Chemische Berichte, 1892 , vol. 25, p. 2623
Journal of the Chemical Society, 1919 , vol. 115, p. 1071
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Tscherniac; Hellon
Chemische Berichte, 1883 , vol. 16, p. 349
