2.3.4.5.6-五氯苯甲腈合成路线 (共 34 条)
反应条件
potassium fluoride; potassium hydroxide in benzonitrile T=315°C; 18 h;
参考文献
Nippon Shokubai Co., Ltd.
Patent: US6392084 B1, 2002 ;
Location in patent: Page column 14 ;
反应条件
potassium fluoride in benzonitrile T=320 - 340°C; 12 - 18 h; Product distribution / selectivity;
参考文献
JP2005/112745 A, ;
Page/Page column 8-9 ;
反应条件
heating to 300°C, 40 h in autoclave; distn.;
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 1341 - 1342
反应条件
heating to 350°C, 20 h in autoclave; distn.;
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 1341 - 1342
反应条件
2: H2SO4 View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
反应条件
2: Na2CO3 / not given View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
反应条件
2: N,N-dimethyl acetamide View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
反应条件
2: further solvent(s) View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
反应条件
heating to 300°C, 40 h in autoclave; distn.;
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
反应条件
heating to 350°C, 20 h in autoclave; distn.;
参考文献
Birchall, J. M.; Haszeldine, R. N.; Jones, M. E.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 1341 - 1342