2,6-二氯苯基-4-硝基苯醚合成路线 (共 3 条)
反应条件
potassium hydroxide in N,N-dimethyl acetamide
T=160°C; 6 h;
参考文献
Cremlyn, Richard; Montgomery, Stephen; Ng, Yew; Simpson, David
Phosphorus and Sulfur and the Related Elements, 1981 , vol. 12, p. 341 - 352
反应条件
in dimethyl sulfoxide
T=90°C; 15 h;
参考文献
Sammes, P. G.; Thetford, D.; Voyle, M.
Journal of the Chemical Society, Chemical Communications, 1987 , # 18 p. 1373 - 1374
反应条件
1: 1.) MeOH, Na / 2.) room t.
2: 71 percent / dimethylsulfoxide / 15 h / 90 °C
View Scheme
参考文献
Sammes, Peter G.; Thetford, Dean; Voyle, Martyn
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3229 - 3232