potassium tert-butylate in dimethyl sulfoxide T=100 - 105°C; 6 h;

1: 55 mg / pyridine, tetramethylammonium hydroxide / H2O / 40 h / Heating 2: 85 mg / boron trichloride / CH2Cl2 / 1) o-5 deg C, 3 h; 2) 5 deg C --> room temperature, 1 h 3: potassium carbonate / acetone / 1 h / Heating 4: potassium t-butoxide / dimethylsulfoxide / 6 h / 100 - 105 °C View Scheme

1: potassium carbonate / acetone / 1 h / Heating 2: potassium t-butoxide / dimethylsulfoxide / 6 h / 100 - 105 °C View Scheme

1: 980 mg / 1,5-diazabicyclo<5.4.0>undec-5-ene / benzene / 10 h / Heating 2: potassium t-butoxide / dimethylsulfoxide / 6 h / 100 - 105 °C View Scheme

1: 85 mg / boron trichloride / CH2Cl2 / 1) o-5 deg C, 3 h; 2) 5 deg C --> room temperature, 1 h 2: potassium carbonate / acetone / 1 h / Heating 3: potassium t-butoxide / dimethylsulfoxide / 6 h / 100 - 105 °C View Scheme

methanol; potassium hydroxide