1,1′-偶氮双(环己烷甲腈)合成路线 （共 17 条）
反应条件
N-bromosuccinmide in tetrachloromethane
参考文献
Chen, Gang; Crawford, Jason; Skerlj, Renato
Patent: US2005/154201 A1, 2005 ;
反应条件
in n-heptane
T=95°C; 36 h; Inert atmosphere;
参考文献
Pal, Ayan; Salandria, Kerry J.; Arico, Joseph W.; Schlegel, Mark K.; McLaughlin, Larry W.
Chemical Communications, 2013 , vol. 49, # 28 p. 2936 - 2938
反应条件
1: Et3SnH / toluene
2: aq. HCl
View Scheme
参考文献
Neumann,W.P. et al.
Justus Liebigs Annalen der Chemie, 1965 , vol. 688, p. 14 - 27
反应条件
in not given
byproducts: C2H6, N2, cyclo-C6H11CN; reaction at 100°C; reaction mechanism discussed;;
参考文献
Neumann, W. P.; Sommer, R.; Lind, H.
Liebigs Annalen der Chemie, 1965 , vol. 688, p. 14 - 27
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.2.4.4, page 32 - 34
反应条件
acetic acid in C6H5Cl
参考文献
Massachusetts Institute of Technology
Patent: US7399639 B2, 2008 ;
反应条件
in not given
byproducts: C2H6, N2, cyclo-C6H11CN; reaction at 100°C; reaction mechanism discussed;;
参考文献
Neumann, W. P.; Sommer, R.; Lind, H.
Liebigs Annalen der Chemie, 1965 , vol. 688, p. 14 - 27
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.2.4.4, page 32 - 34
反应条件
Triethylzinnwasserstoff in toluene
参考文献
Neumann,W.P. et al.
Justus Liebigs Annalen der Chemie, 1965 , vol. 688, p. 14 - 27
