1-苯基-2,8,9-三氧杂-5-氮杂-1-硅杂二环[3.3.3]十一烷合成路线 （共 44 条）
反应条件
in tetrahydrofuran
1 h; Heating;
参考文献
Bedard, Thomas C.; Corey, Joyce Y.
Journal of Organometallic Chemistry, 1992 , vol. 428, # 3 p. 315 - 333
反应条件
in chloroform
T=20°C; 96 h;
参考文献
Voronkov, M. G.; Pestunovich, V. A.; Petukhov, L. P.; Rakhlin, V. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 3 p. 637
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 3 p. 699
反应条件
1: LiAlH4 / diethyl ether / Heating
2: dicobalt octacarbonyl / CH2Cl2 / Ambient temperature
View Scheme
参考文献
Hosomi, Akira; Iijima, Susumu; Sakurai, Hideki
Chemistry Letters, 1981 , p. 243 - 246
反应条件
in para-xylene
T=-5 - 0°C; 0.666667 h;
参考文献
Voronkov; Albanov; Grebneva; Trofimova; Chernov; Chipanina
Russian Journal of General Chemistry, 2006 , vol. 76, # 12 p. 1854 - 1859
反应条件
in chloroform
T=0 - 20°C; Inert atmosphere;
参考文献
Voronkov; Kuznetsova
Russian Journal of General Chemistry, 2009 , vol. 79, # 5 p. 925 - 927
反应条件
T=140 - 150°C; Yields of byproduct given;
参考文献
Voronkov, M. G.; Kuznetsova, G. A.; Baryshok, V. P.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 7 p. 1682,1512 - 1513
反应条件
1: heptafluoroiodopropane / acetonitrile / 0.5 h / 20 °C / Irradiation
2: CH2Cl2 / 96 h / 30 °C
View Scheme
参考文献
Voronkov, M. G.; Baryshok, V. P.; Petukhov, L. P.; Rakhlin, V. I.; Mirskov, R. G.; Pestunovich, V. A.
Journal of Organometallic Chemistry, 1988 , vol. 358, p. 39 - 56
反应条件
1: 15 percent / iodine / CH2Cl2 / -60 °C
2: CH2Cl2 / 96 h / 30 °C
View Scheme
参考文献
Voronkov, M. G.; Baryshok, V. P.; Petukhov, L. P.; Rakhlin, V. I.; Mirskov, R. G.; Pestunovich, V. A.
Journal of Organometallic Chemistry, 1988 , vol. 358, p. 39 - 56
反应条件
dicobalt octacarbonyl in dichloromethane
Ambient temperature;
参考文献
Hosomi, Akira; Iijima, Susumu; Sakurai, Hideki
Chemistry Letters, 1981 , p. 243 - 246
反应条件
potassium hydroxide in benzene
Heating;
参考文献
Hosomi, Akira; Iijima, Susumu; Sakurai, Hideki
Chemistry Letters, 1981 , p. 243 - 246
