1-苯基-2,8,9-三氧杂-5-氮杂-1-硅杂二环[3.3.3]十一烷合成路线 (共 44 条)
反应条件
potassium hydroxide in xylene
参考文献
Voronkov,M.G.; Zelchan,G.I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1965 , vol. 1, p. 33 - 37
Khimiya Geterotsiklicheskikh Soedinenii, 1965 , vol. 1, p. 51 - 57
反应条件
1: 81 percent / pyridine / diethyl ether / 2 h / Heating
2: 42 percent / acetonitrile; xylene / 10 h / Heating
View Scheme
参考文献
Grobe, Joseph; Henkel, Gerald; Krebs, Bernt; Voulgarakis, Nikolaos
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1984 , vol. 39, # 3 p. 341 - 351
反应条件
in acetonitrile; xylene
10 h; Heating;
参考文献
Grobe, Joseph; Henkel, Gerald; Krebs, Bernt; Voulgarakis, Nikolaos
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1984 , vol. 39, # 3 p. 341 - 351
反应条件
tetrabutyl ammonium fluoride; triphenylphosphine; palladium diacetate in tetrahydrofuran; N,N-dimethyl-formamide
Heating;
参考文献
Riggleman, Shaundra; DeShong, Philip
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8106 - 8109