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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
20973-67-5
合成路线
(共 8 条)
20973-67-5
→
反应条件
150760-45-5
2-(2,2-二甲氧基乙基)苯甲酰胺
反应条件
1: camphorsulfonic acid / 9 h / Heating 2: 97 percent / H2 / Pd/C / ethanol / Ambient temperature View Scheme
参考文献
Arai, Eri; Tokuyama, Hidetoshi; Linsell, Martin S.; Fukuyama, Tohru
Tetrahedron Letters, 1998 , vol. 39, # 1-2 p. 71 - 74
20973-67-5
→
反应条件
201486-54-6
反应条件
1: camphorsulfonic acid / 9 h / Heating 2: 97 percent / H2 / Pd/C / ethanol / Ambient temperature 3: 84 percent / pyridine / 1 h / Ambient temperature 4: 82 percent / PPTS / benzene / 2 h / Heating View Scheme
参考文献
Arai, Eri; Tokuyama, Hidetoshi; Linsell, Martin S.; Fukuyama, Tohru
Tetrahedron Letters, 1998 , vol. 39, # 1-2 p. 71 - 74
20973-67-5
→
反应条件
552-89-6
邻硝基苯甲醛
反应条件
dihydrogen peroxide in acetonitrile T=25°C; 4 h;
参考文献
Dai, Liyan; Yu, Jie; Chen, Yingqi; Yu, Shichao
Synthetic Communications, 2011 , vol. 41, # 20 p. 3078 - 3084
20973-67-5
→
反应条件
3289-82-5
反应条件
ammonium chloride; zinc in diethyl ether; water Reduction; 8 h;
参考文献
Vo, Quan V.; Trenerry, Craige; Rochfort, Simone; Wadeson, Jenny; Leyton, Carolina; Hughes, Andrew B.
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 2 p. 856 - 864
20973-67-5
→
反应条件
67282-55-7
1-甲氧基-1H-吲哚-3-甲醛
反应条件
1.1: water; zinc; ammonium chloride / diethyl ether / 4 h / 20 °C 2.1: Aliquatreg; 336; sodium hydroxide / diethyl ether; water / 21 h / 20 °C 3.1: trichlorophosphate / |Cooling with ice 3.2: 3 h / 20 °C 3.3: |Cooling with ice View Scheme
参考文献
Vo, Quan V.; Trenerry, Craige; Rochfort, Simone; Wadeson, Jenny; Leyton, Carolina; Hughes, Andrew B.
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 2 p. 856 - 864
20973-67-5
→
反应条件
69111-76-8
反应条件
1.1: water; zinc; ammonium chloride / diethyl ether / 4 h / 20 °C 2.1: Aliquatreg; 336; sodium hydroxide / diethyl ether; water / 21 h / 20 °C 3.1: trichlorophosphate / |Cooling with ice 3.2: 3 h / 20 °C 3.3: |Cooling with ice 4.1: ammonium acetate / 2 h / |Reflux View Scheme
参考文献
Vo, Quan V.; Trenerry, Craige; Rochfort, Simone; Wadeson, Jenny; Leyton, Carolina; Hughes, Andrew B.
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 2 p. 856 - 864
67-56-1
甲醇
+
20973-67-5
→
反应条件
79844-33-0
反应条件
camphor-10-sulfonic acid 9 h; Heating; Yield given;
参考文献
Arai, Eri; Tokuyama, Hidetoshi; Linsell, Martin S.; Fukuyama, Tohru
Tetrahedron Letters, 1998 , vol. 39, # 1-2 p. 71 - 74
20973-67-5
→
反应条件
54698-11-2
1-甲氧基-1H-吲哚
反应条件
1: water; zinc; ammonium chloride / diethyl ether / 4 h / 20 °C 2: Aliquatreg; 336; sodium hydroxide / diethyl ether; water / 21 h / 20 °C View Scheme
参考文献
Vo, Quan V.; Trenerry, Craige; Rochfort, Simone; Wadeson, Jenny; Leyton, Carolina; Hughes, Andrew B.
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 2 p. 856 - 864