(S)-(+)-2-苯甘氨醇合成路线 （共 103 条）
反应条件
chlorosulfonic acid; sodium hydroxide
参考文献
Buckley, Benjamin R.; Patel, Anish P.; Wijayantha
Journal of Organic Chemistry, 2013 , vol. 78, # 3 p. 1289 - 1292
反应条件
tetrachloromethane; triethylamine; triphenylphosphine in pyridine; acetonitrile
Ambient temperature; Yields of byproduct given;
参考文献
Vorbrueggen, Helmut; Krolikiewicz, Konrad
Tetrahedron Letters, 1981 , vol. 22, # 45 p. 4471 - 4474
反应条件
C29H46IrN5P2; potassium tert-butylate in tetrahydrofuran
T=90°C; 24 h;
参考文献
Qu, Shuanglin; Dang, Yanfeng; Song, Chunyu; Wen, Mingwei; Huang, Kuo-Wei; Wang, Zhi-Xiang
Journal of the American Chemical Society, 2014 , vol. 136, # 13 p. 4974 - 4991
反应条件
in nitromethane
0.0833333 h; microwave irradiation;
参考文献
Bratulescu, George
Synthesis, 2007 , # 20 p. 3111 - 3112
反应条件
1: 89 percent / pyridine / tetrahydrofuran / 3 h / -15 °C
2: 90 percent / NaOCH3 / tetrahydrofuran / 12 h / Ambient temperature
View Scheme
参考文献
Pirkle, William H.; Simmons, Kirk A.
Journal of Organic Chemistry, 1983 , vol. 48, # 15 p. 2520 - 2527
参考文献
Mallesham; Rajesh; Reddy, P Rajamohan; Srinivas; Trehan, Sanjay
Organic letters, 2003 , vol. 5, # 7 p. 963 - 965
反应条件
tributylphosphine; bis-o-nitrothiophenol; oxygen; triethylamine
10 h;
参考文献
Kodaka, Masato; Tomohiro, Takenori; Lee, Ah Lek; Okuno, Hiroaki(Yohmei)
Journal of the Chemical Society, Chemical Communications, 1989 , # 19 p. 1479 - 1481
反应条件
toluene-4-sulfonic acid in benzene
T=20°C; 12 h;
参考文献
David, Olivier; Calvet, Sandrine; Chau, Francois; Vanucci-Bacque, Corinne; Fargeau-Bellassoued, Marie-Claude; Lhommet, Gerard
Journal of Organic Chemistry, 2004 , vol. 69, # 8 p. 2888 - 2891
反应条件
1: 4 h / 65 °C
2: Bu2SnClH; HMPA / tetrahydrofuran / 2.5 h / 0 °C
View Scheme
参考文献
Suwa, Toshihiro; Sugiyama, Erika; Shibata, Ikuya; Baba, Akio
Synthesis, 2000 , # 6 p. 789 - 800
反应条件
1: toluene
2: sodium tetrahydroborate / methanol / 20 - 45 °C
View Scheme
参考文献
Gudaprthi, Vijayalakshmi; Bharathi; Omprakash
Asian Journal of Chemistry, 2011 , vol. 23, # 2 p. 765 - 769
