2-苯基-3-甲基环氮丙啶合成路线 （共 6 条）
反应条件
trifluoroacetic acid in dichloromethane; acetonitrile T=-78°C; Addition;
参考文献
Ho, Chi-Ming; Lau, Tai-Chu; Kwong, Hoi-Lun; Wong, Wing-Tak
Journal of the Chemical Society - Dalton Transactions, 1999 , # 15 p. 2411 - 2413
反应条件
trifluoroacetic acid; manganese nitrido in dichloromethane; acetonitrile T=-78°C; Addition; Product distribution; Further Variations:CatalystsReaction partnersReagents;
参考文献
Ho, Chi-Ming; Lau, Tai-Chu; Kwong, Hoi-Lun; Wong, Wing-Tak
Journal of the Chemical Society - Dalton Transactions, 1999 , # 15 p. 2411 - 2413
反应条件
1: 2.) aq. sodium bisulphite / 1.) dichloromethane, reflux, 1 h 2.) 10 deg C 2: 97.5 percent / sodium ethoxide / CH2Cl2 / 1 h / Ambient temperature 3: LAH / diethyl ether / 1.5 h / Ambient temperature View Scheme
参考文献
Zawadzki, S.; Zwierzak, A.
Tetrahedron, 1981 , vol. 37, # 15 p. 2675 - 2681
反应条件
1: 93 percent 2: 49 percent / AIBN, 1.6 eq. Bu3SnH / benzene / 0.5 h / Heating View Scheme
参考文献
Werry, Juergen; Stamm, Helmut; Lin, Pen-Yuan; Falkenstein, Reinhard; Gries, Stefan; Irngartinger, Hermann
Tetrahedron, 1989 , vol. 45, # 16 p. 5015 - 5028
反应条件
palladium on activated charcoal; hydrogen in methanol T=20°C; 16 h;
参考文献
Jat, Jawahar L.; Paudyal, Mahesh P.; Gao, Hongyin; Xu, Qing-Long; Yousufuddin, Muhammed; Devarajan, Deepa; Ess, Daniel H.; Kurti, Laszlo; Falck, John R.
Science, 2014 , vol. 343, # 6166 p. 61 - 65
反应条件
palladium on activated charcoal; hydrogen in methanol T=20°C; 16 h;
参考文献
Jat, Jawahar L.; Paudyal, Mahesh P.; Gao, Hongyin; Xu, Qing-Long; Yousufuddin, Muhammed; Devarajan, Deepa; Ess, Daniel H.; Kurti, Laszlo; Falck, John R.
Science, 2014 , vol. 343, # 6166 p. 61 - 65
