5,7-二氢-5-甲基-6H-二苯并[b,d]氮杂卓-6-酮合成路线 (共 12 条)
反应条件
1: With potassium tert-butylate; isopentyl nitrite 2: With acetic acid; zinc in methanol
参考文献
Cole, Kevin P.; Mitchell, David; Austin Carr; Stout, James R.; Belvo, Matthew D.
Tetrahedron Asymmetry, 2009 , vol. 20, # 11 p. 1262 - 1266
反应条件
1: With potassium hexamethylsilazane; isopentyl nitrite in toluene T=0°C; 1 h; 2: With hydrogen; palladium on activated charcoal in ethanol T=20°C; P=1800.18 Torr; 24 h; Further stages.;
参考文献
Peters, Jens-Uwe; Galley, Guido; Jacobsen, Helmut; Czech, Christian; David-Pierson, Pascale; Kitas, Eric A.; Ozmen, Laurence
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 21 p. 5918 - 5923