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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
21003-53-2
合成路线
（共 11 条）
4784-77-4
1-溴-2-丁烯
+
5720-05-8
4-甲基苯硼酸
→
反应条件
21003-53-2
反应条件
aluminum oxide; potassium fluoride; palladium T=100°C; Suzuki reaction; 4 h;
参考文献
Kabalka, George W.; Wang, Lei; Pagni, Richard M.; Hair, C. Maxwell; Namboodiri, Vasudevan
Synthesis, 2003 , # 2 p. 217 - 222
106-99-0
丁二烯
+
4294-57-9
对甲苯基溴化镁
→
反应条件
33356-85-3
+
21003-53-2
+
20574-99-6
4-(4-甲基苯基)-1-丁烯
反应条件
iron(III) chloride; potassium carbonate in tetrahydrofuran; diethyl ether T=10 - 15°C; 18 h;
参考文献
Zubritskii, L. M.; Romashchenkova, N. D.; Petrov, A. A.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2157 - 2167
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 12 p. 2465 - 2477
124745-26-2
→
反应条件
21003-53-2
+
79211-50-0
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane; water T=60°C; Yield given. Title compound not separated from byproducts;
参考文献
Baudin, Jean-Bernard; Julia, Silvestre A.
Tetrahedron Letters, 1989 , vol. 30, # 15 p. 1967 - 1970
124745-27-3
→
反应条件
21003-53-2
+
79211-50-0
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane; water T=60°C; Yield given. Title compound not separated from byproducts;
参考文献
Baudin, Jean-Bernard; Julia, Silvestre A.
Tetrahedron Letters, 1989 , vol. 30, # 15 p. 1967 - 1970
563-52-0
3-氯-1-丁烯
+
108-88-3
甲苯
→
反应条件
21003-53-2
+
34136-20-4
反应条件
indium; 4 Angstroem MS; calcium carbonate in xylene T=80°C; 3 h; Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Lim, Hwan Jung; Keum, Gyochang; Kang, Soon Bang; Kim, Youseung; Chung, Bong Young
Tetrahedron Letters, 1999 , vol. 40, # 8 p. 1547 - 1550
4894-61-5
(E)-巴豆氯
+
108-88-3
甲苯
→
反应条件
21003-53-2
+
34136-20-4
反应条件
indium; 4 Angstroem MS; calcium carbonate in xylene T=80°C; 3 h; Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Lim, Hwan Jung; Keum, Gyochang; Kang, Soon Bang; Kim, Youseung; Chung, Bong Young
Tetrahedron Letters, 1999 , vol. 40, # 8 p. 1547 - 1550
→
反应条件
21003-53-2
反应条件
Fe(acac)3 in ethylene glycol dimethyl ether T=25°C; 4 h; Inert atmosphere; optical yield given as percent deregioselective reaction;
参考文献
Volla, Chandra M. R.; Markovic, Dean; Dubbaka, Srinivas Reddy; Vogel, Pierre
European Journal of Organic Chemistry, 2009 , # 36 p. 6281 - 6288
86739-16-4
+
4294-57-9
对甲苯基溴化镁
→
反应条件
21003-53-2
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in diethyl ether 26 h; Ambient temperature;
参考文献
Hayashi, Tamio; Konishi, Mitsuo; Yokota, Kan-Ichi; Kumada, Makoto
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 359 - 374
4894-61-5
(E)-巴豆氯
+
108-88-3
甲苯
→
反应条件
21003-53-2
+
34136-20-4
反应条件
Pb3BrF5 2 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ichihara, Junko
Chemical Communications, 1997 , # 19 p. 1921 - 1922
563-52-0
3-氯-1-丁烯
+
108-88-3
甲苯
→
反应条件
21003-53-2
+
34136-20-4
反应条件
Pb3BrF5 2 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ichihara, Junko
Chemical Communications, 1997 , # 19 p. 1921 - 1922
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