1-叠氮基-4-甲氧基苯合成路线 (共 93 条)
反应条件
poly(styrene-co-3-maleimidophenyldiphenylphosphine) in tetrahydrofuran
T=20°C; 22 h;
参考文献
Mahdavi, Hossein; Amani, Javad
Tetrahedron Letters, 2009 , vol. 50, # 43 p. 5923 - 5926
反应条件
5,10,15,20-tetraphenyl-21H,23H-porphine Co(II)
2 h; Heating;
参考文献
Cenini; Gallo; Penoni; Ragaini; Tollari
Chemical Communications, 2000 , # 22 p. 2265 - 2266
反应条件
1: tetrahydrofuran / 3 h / 20 °C
2: tetrahydrofuran / 3 h / Heating
View Scheme
参考文献
Hemming; Bevan; Loukou; Patel; Renaudeau
Synlett, 2000 , # 11 p. 1565 - 1568
参考文献
Prodanchuk, N. G.; Megera, I. V.; Patratii, V. K.
Pharmaceutical Chemistry Journal, 1984 , vol. 18, # 2 p. 108 - 110
Khimiko-Farmatsevticheskii Zhurnal, 1984 , vol. 18, # 2 p. 173 - 175
反应条件
in benzene
15 h; Heating;
参考文献
Markova, N. K.; Tsil'ko, A. E.; Galishev, V. A.; Maretina, I. A.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 1990 - 1993
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 11 p. 2281 - 2285
反应条件
Ru(II)[meso-tetraphenylporphyrin](CO)
7 h; Inert atmosphereReflux;
参考文献
Intrieri, Daniela; Caselli, Alessandro; Ragaini, Fabio; MacChi, Piero; Casati, Nicola; Gallo, Emma
European Journal of Inorganic Chemistry, 2012 , # 3 p. 569 - 580
反应条件
ammonium hydroxide; iron in methanol
T=25°C; Reduction; condensation; 1 h; sonication;
参考文献
Chandrasekhar; Narsihmulu
Tetrahedron Letters, 2000 , vol. 41, # 41 p. 7969 - 7972
反应条件
1: acetylenecarboxylic acid With 2-nitrobenzeneboronic acid in 1,2-dichloro-ethane
T=25°C; 0.166667 h; Inert atmosphere;
2: 4-Methoxyphenylazide in 1,2-dichloro-ethane
T=25°C; Huisgen cycloaddition; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Benbayer, Chahinez; Kheddam, Narimane; Saidi-Besbes, Salima; Givenchy, Elisabeth Taffin De; Guittard, Frederic; Grelet, Eric; Safer, Abdel Mounaim; Derdour, Aicha
Journal of Molecular Structure, 2013 , vol. 1034, p. 22 - 28
反应条件
1.1: copper(II) sulfate; sodium L-ascorbate; BPDS / water; N,N-dimethyl-formamide / 0 - 20 °C / |Inert atmosphere
2.1: sodium hydroxide / water; methanol / 20 °C / |Inert atmosphere
2.2: pH 5 - Ca. 6 / |Inert atmosphere
View Scheme
参考文献
Bai, Suping; Li, Shihong; Xu, Jinbin; Peng, Xin; Sai, Kiran; Chu, Wenhua; Tu, Zhude; Zeng, Chenbo; Mach, Robert H.
Journal of Medicinal Chemistry, 2014 , vol. 57, # 10 p. 4239 - 4251
反应条件
in various solvent(s)
T=155°C; 8 h;
参考文献
Nay, Barry; Scriven, Eric F. V.; Suschitzky, Hans; Thomas, Desmond R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 611 - 613