1-AZIDO-3-BROMOBENZENE SOLUTION合成路线 （共 8 条）
反应条件
1: With hydrogenchloride in water T=0 - 5°C; 0.5 h; 2: With sodium azide; sodium nitrite in water T=0 - 5°C; 1 h;
参考文献
Berger, Olivier; Kaniti, Archana; van Ba, Christophe Tran; Vial, Henri; Ward, Stephen A.; Biagini, Giancarlo A.; Bray, Patrick G.; O'Neill, Paul M.
ChemMedChem, 2011 , vol. 6, # 11 p. 2094 - 2108
反应条件
sodium azide; copper ferrite in water T=20°C; 7 h;
参考文献
Kumar, A. Suresh; Reddy, M. Amarnath; Knorn; Reiser; Sreedhar
European Journal of Organic Chemistry, 2013 , # 21 p. 4674 - 4680
反应条件
copper(l) iodide; sodium azide; sodium L-ascorbate; trans-N,N'-dimethylcyclohexane-1,2-diamine in ethanol 0.5 h; Heating;
参考文献
Andersen, Jacob; Madsen, Ulf; Bjoerkling, Fredrik; Liang, Xifu
Synlett, 2005 , # 14 art. no. D17405ST, p. 2209 - 2213
参考文献
Spauschus; Scott
Journal of the American Chemical Society, 1951 , vol. 73, p. 208
反应条件
trifluorormethanesulfonic acid; trifluoroacetic acid T=25°C; 4 h;
参考文献
Journal of Chemical Research, Miniprint, , # 12 p. 3156 - 3188
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate
1.) DME, 10 min, 2.) DME, reflux, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Wellmar, Ulf; Hoernfeldt, Anna-Britta; Gronowitz, Salo
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 2 p. 409 - 414
反应条件
1: in dimethyl sulfoxide
T=20°C; 0.25 h;
2: With water in dimethyl sulfoxide
参考文献
Jiang, Yubo; Kuang, Chunxiang; Yang, Qing
Tetrahedron, 2011 , vol. 67, # 2 p. 289 - 292
反应条件
copper(l) iodide; triethylamine in dimethyl sulfoxide
T=20°C; P=760.051 Torr; 24 h;
参考文献
Wu, Lu-Yong; Xie, Yong-Xin; Chen, Zi-Sheng; Niu, Yan-Ning; Liang, Yong-Min
Synlett, 2009 , # 9 p. 1453 - 1456
