(9CI)-3,5-二氟吡啶 1-氧化物合成路线 （共 3 条）
反应条件
peracetic acid in chloroform; acetic acid T=50°C; 24 h;
参考文献
Chambers, Richard D.; Hall, Christopher W.; Hutchinson, John; Millar, Ross W.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 10 p. 1705 - 1713
反应条件
1: 30 percent Chromat. / LiAlH4 / diethyl ether / 28 h / 0 - 20 °C 2: 71 percent / peracetic acid / CHCl3; acetic acid / 24 h / 50 °C View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 10 p. 1705 - 1713
反应条件
1: 63 percent / H2, Et3N / Pd/C / CH2Cl2 / 21 h / 3000.2 Torr / Ambient temperature 2: 71 percent / peracetic acid / CHCl3; acetic acid / 24 h / 50 °C View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 10 p. 1705 - 1713
