2,3,4-三甲氧基苯甲醛合成路线 （共 87 条）
反应条件
sodium hydroxide anschliessend in einer Wasserstoff-Atmosphaere;
参考文献
Journal of the Chemical Society, , vol. 97, p. 2260
反应条件
1: HCl; ZnCl2; diethyl ether / Erhitzen des Reaktionsprodukts mit Wasser 2: aqueous alkaline solution View Scheme
参考文献
Journal of the Chemical Society, , p. 2542,2544
参考文献
Journal of the Chemical Society, , p. 2542,2544
反应条件
potassium carbonate; acetone
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 145, p. 313,315
反应条件
1: NH4OAc / acetic acid / Heating 2: LiAlH4 View Scheme
参考文献
Shulgin
Journal of medicinal chemistry, 1966 , vol. 9, # 3 p. 445 - 446
反应条件
1: boron trichloride / dichloromethane / 20 h / 20 °C / Inert atmosphere 2: 4-(N,N-dimethlyamino)pyridine; triethylamine / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere View Scheme
参考文献
Beale, Thomas M.; Bond, Peter J.; Brenton, James D.; Charnock-Jones, D. Stephen; Ley, Steven V.; Myers, Rebecca M.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 5 p. 1749 - 1759
反应条件
1: 1.) NaOMe, 2.) H2 / 2.) Pd-C / 1.) MeOH, -10 deg C, 3h, 2.) AcOEt, 20 deg C, 6h 2: HCl / 1 h / 20 °C View Scheme
参考文献
Landais; Robin; Lebrun
Tetrahedron, 1991 , vol. 47, # 23 p. 3787 - 3804
反应条件
in tetrahydrofuran; chloroform; mineral oil
参考文献
Kowa Co., Ltd.
Patent: US2003/22887 A1, 2003 ;
反应条件
1: With piperidine; pyridine Reflux; 2: With hydrogenchloride in water T=25°C;
参考文献
Chang, Sheng; Yin, Shi-Liang; Wang, Jian; Jing, Yong-Kui; Dong, Jin-Hua
Molecules, 2009 , vol. 14, # 10 p. 4166 - 4179
参考文献
Morinaga Milk Industry Co., Ltd.
Patent: US5574062 A1, 1996 ;
