5-甲酰基噻唑-2-氨基甲酸叔丁酯合成路线 （共 34 条）
反应条件
hydrogenchloride in water
Reflux;
参考文献
Dhakar, Neelam; Ojha, Swati; Jat, Jawahar Lal; Talesara
Journal of the Indian Chemical Society, 2008 , vol. 85, # 6 p. 660 - 664
反应条件
1: acetone / 1 h / Heating
2: 72 percent / aq. NaOH / 0.33 h / Heating
View Scheme
参考文献
Sawhney, S. N.; Dhindsa, G. S.; Singh, S. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 10 p. 1044 - 1049
反应条件
1: 87 percent / pyridine / Ambient temperature
2: PCl5 / 1.5 h / 130 °C
3: sodium azide, sodium acetate / acetone; H2O / 8 h
4: 50 percent / decahydronaphthalene / 2 h / Heating
View Scheme
参考文献
Ramachandraiah, G.; Reddy, K. Kondal
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 808 - 810
反应条件
in acetone
1 h; Heating;
参考文献
Dhindsa, G. S.
Polish Journal of Chemistry, 1986 , vol. 60, # 4-6 p. 609 - 614
反应条件
1.) acetone, reflux, 1 h, 2.) acetone, reflux, 15 min; Yield given. Multistep reaction;
参考文献
Sawhney, S. N.; Dhindsa, G. S.; Singh, S. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 10 p. 1044 - 1049
反应条件
piperidine in ethanol
1 h; Heating;
参考文献
Dash; Patra; Mahapatra
Journal of the Indian Chemical Society, 1983 , vol. 60, # 8 p. 772 - 774
反应条件
1: potassium carbonate / toluene / 24 h / 20 °C / |Reflux
2: toluene / |Reflux
View Scheme
参考文献
Hassan, Ghada S.; El-Messery, Shahenda M.; Al-Omary, Fatmah A.M.; El-Subbagh, Hussein I.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 20 p. 6318 - 6323
反应条件
in benzene
3 h; Heating;
参考文献
Liu, Hui-Ling; Li, Zongcheng; Anthonsen, Thorleif
Molecules, 2000 , vol. 5, # 9 p. 1055 - 1061
反应条件
1: 81 percent / pyridine / Ambient temperature
2: PCl5 / 1.5 h / 130 °C
View Scheme
参考文献
Ramachandraiah, G.; Reddy, K. Kondal
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 808 - 810
反应条件
hydrogenchloride; sodium acetate; sodium nitrite
1.) water, 0 deg C; 2.) water, ethanol, 2 h; Yield given. Multistep reaction;
参考文献
Rao; Khan; Mehra
Journal of the Indian Chemical Society, 1982 , vol. 59, # 3 p. 375 - 377
