2-[(甲氨基)甲基]吡啶合成路线 (共 15 条)
反应条件
sodium tetrahydroborate in methanol 3 h; Yield given;
参考文献
Magnetic Resonance in Chemistry, , vol. 25, p. 696 - 706
反应条件
sodium cyanoborohydride in methanol 72 h; Ambient temperature; Yield given;
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 320, # 7 p. 647 - 654
反应条件
cis-[Ru(dimethyl sulfoxide)4Cl2]; phenyl silane; di-(1-adamantyl)-n-butylphosphine in toluene T=100°C; P=22502.3 Torr; AutoclaveInert atmosphere;
参考文献
Li, Yuehui; Fang, Xianjie; Junge, Kathrin; Beller, Matthias
Angewandte Chemie - International Edition, 2013 , vol. 52, # 36 p. 9568 - 9571
Angew. Chem., 2013 , vol. 125, # 36 p. 9747 - 9750,4
反应条件
hydrogen; platinum(IV) oxide in acetic acid P=3102.9 Torr;
参考文献
Banting, Lee; Crabb, Trevor A.
Magnetic Resonance in Chemistry, 1987 , vol. 25, p. 696 - 706
反应条件
1: Heating 2: 1.) n-BuLi / 1.) THF, -78 deg C, 1.5 h, 2.) -78 deg C-room temp. 3: hydrazine hydrate / ethanol; acetic acid / 25 °C View Scheme
参考文献
Meyers; Marra
Tetrahedron Letters, 1985 , vol. 26, # 48 p. 5863 - 5866