1H-吡啶并[2,3-d][1,3]噁嗪-2,4-二酮合成路线 （共 18 条）
反应条件
sodium hydride in N,N-dimethyl-formamide 3 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 43, # 4 p. 663 - 668
反应条件
sodium hydride 1) dimethylacetamide, RT, 1h, 60 deg C, 30 min, 2) RT, 4 h; Yield given. Multistep reaction;
参考文献
Journal of Heterocyclic Chemistry, , vol. 22, p. 193 - 206
反应条件
sodium hydride 1) dimethylacetamide, RT, 1h, 60 deg C, 30 min, 2) RT, 4 h; Yield given. Multistep reaction;
参考文献
Coppola, Gary M.; Fraser, James D.; Hardtmann, Goetz E.; Shapiro, Michael J.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 193 - 206
反应条件
sodium hydride 1) dimethylacetamide, RT, 1h, 60 deg C, 30 min, 2) RT, 4 h; Yield given. Multistep reaction;
参考文献
Coppola, Gary M.; Fraser, James D.; Hardtmann, Goetz E.; Shapiro, Michael J.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 193 - 206
反应条件
1: 1) NaH / 1) dimethylacetamide, RT, 1h, 60 deg C, 30 min, 2) RT, 4 h 2: 1) NaH / 1) dimethylacetamide, 2) 120 deg C, 18 h View Scheme
参考文献
Coppola, Gary M.; Fraser, James D.; Hardtmann, Goetz E.; Shapiro, Michael J.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 193 - 206
反应条件
sodium hydride in N,N-dimethyl-formamide 3 h; Ambient temperature;
参考文献
Canonne, P.; Boulanger, R.; Chantegrel, B.
Tetrahedron, 1987 , vol. 43, # 4 p. 663 - 668
反应条件
sodium hydride
1) dimethylacetamide, RT, 1h, 2) 60 deg C, 30 min, 3) RT, 4 h; Yield given. Multistep reaction;
参考文献
Coppola, Gary M.; Fraser, James D.; Hardtmann, Goetz E.; Shapiro, Michael J.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 193 - 206
反应条件
1: 1) NaH / 1) dimethylacetamide, RT, 1h, 60 deg C, 30 min, 2) RT, 4 h
2: 1) NaH / 1) dimethylacetamide, RT, 30 min, 2) 120 deg C, 18 h
View Scheme
参考文献
Coppola, Gary M.; Fraser, James D.; Hardtmann, Goetz E.; Shapiro, Michael J.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 193 - 206
