potassium hydroxide in methanol T=45°C; electrolysis: anode: platinum foil; current source: galvanostat; current density 220 mA cm-2; current consumption: 1.4 F mol-1; cell voltage 20 V; Yield given;
1: triethylamine / tetrahydrofuran / 1 h / -5 °C 2: sodium tetrahydroborate / water / 1 h / 0 °C 3: triethylamine / dichloromethane / 1 h / 0 °C View Scheme
参考文献
Von Delius, Max; Geertsema, Edzard M.; Leigh, David A.; Tang, Dan-Tam D.
Journal of the American Chemical Society, 2010 , vol. 132, # 45 p. 16134 - 16145
Milburn; Truter
Journal of the Chemical Society, 1954 , p. 3344,3347
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Hougen et al.
Journal of the Chemical Society, 1953 , p. 98,101
