1: methylmalonic acid dimethyl ester With sodium hydride in tetrahydrofuran
2: trans-cinnamyl acetate With [Mo(C7H7)(CO)3]; N,N'-((1S,2S)-cyclohexane-1,2-diyl)dipicolinamide in tetrahydrofuran
T=48°C; Further stages.;
参考文献
Hughes, David L.; Palucki, Michael; Yasuda, Nobuyoshi; Reamer, Robert A.; Reider, Paul J.
Journal of Organic Chemistry, 2002 , vol. 67, # 9 p. 2762 - 2768
benzenesulfonamide; potassium acetate; bis(η3-allyl-μ-chloropalladium(II)); (R,R)-taddol-phosphite-((S)-4-tBu-oxazoline) derivative in dichloromethane
T=20°C; 20 h; Title compound not separated from byproducts;