2-氯甲基-1,4-二氧杂烷合成路线 （共 10 条）
参考文献
Magyar Tudomanvos Akademia Kozponti Kemiai Kutato Intezete Nitrokemia Inartelenek Fuzfogyartelep
Patent: US5116402 A1, 1992 ;
反应条件
phosphorus trichoride
参考文献
Tsivunin, V. S.; Zaripova, V. G.; Bikulova, V. Zh.; Zykova, V. V.; Kapustina, I. V.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 3 p. 580
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 3 p. 660 - 661
反应条件
phosphorus trichoride
参考文献
Tsivunin, V. S.; Zaripova, V. G.; Bikulova, V. Zh.; Zykova, V. V.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 4 p. 938 - 939,826 - 827
反应条件
1: 36 percent / NaOH / H2O / 2 h / 90 °C 2: 50 percent / PCl3 View Scheme
参考文献
Tsivunin, V. S.; Zaripova, V. G.; Bikulova, V. Zh.; Zykova, V. V.; Kapustina, I. V.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 3 p. 580
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 3 p. 660 - 661
反应条件
1: 60 percent / NaOH 2: 36 percent / NaOH / H2O / 2 h / 90 °C 3: 50 percent / PCl3 View Scheme
参考文献
Tsivunin, V. S.; Zaripova, V. G.; Bikulova, V. Zh.; Zykova, V. V.; Kapustina, I. V.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 3 p. 580
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 3 p. 660 - 661
反应条件
1: 80 percent View Scheme
参考文献
Kosary; Kasztreiner; Rabloczky; Vitalis
Pharmazie, 1987 , vol. 42, # 6 p. 373 - 375
反应条件
1: 80 percent 3: 62 percent View Scheme
参考文献
Kosary; Kasztreiner; Rabloczky; Vitalis
Pharmazie, 1987 , vol. 42, # 6 p. 373 - 375
反应条件
1: 69 percent / NaOH, KF / 6 h / 200 - 220 °C
2: 77 percent / PCl5 / CCl4 / Ambient temperature; left overnight
View Scheme
参考文献
Tsivunin, V. S.; Zaripova, V. G.
J. Gen. Chem. USSR (Engl. Transl.), 1984 , vol. 54, # 10 p. 2181 - 2186,1950 - 1954
反应条件
potassium fluoride; sodium hydroxide
T=200 - 220°C; 6 h;
参考文献
Tsivunin, V. S.; Zaripova, V. G.
J. Gen. Chem. USSR (Engl. Transl.), 1984 , vol. 54, # 10 p. 2181 - 2186,1950 - 1954
反应条件
potassium fluoride; sodium hydroxide
T=200 - 220°C; 6 h;
参考文献
Tsivunin, V. S.; Zaripova, V. G.
J. Gen. Chem. USSR (Engl. Transl.), 1984 , vol. 54, # 10 p. 2181 - 2186,1950 - 1954
