CO in methanol; dichloromethane methanol was added under CO to a mixture of the Ru-salt and bis(diphenylphosphino)methane dissolved in CH2Cl2, crystn.; filtn., chromy. on silica gel (CH2Cl2/hexane, 1/4), recrystn. (CH2Cl2/methanol), elem. anal.;
hydrochloric acid in tetrahydrofuran byproducts: hydrogen; soln. of Fe-complex in THF, schlenk flask, addn. of dry HCl gas, filtered, evapn.; H2 detected by GC, react. monitored by IR;
参考文献
Journal of the American Chemical Society, , vol. 111, # 10 p. 3591 - 3597
