反应条件
CF3SO3H in toluene byproducts: Cl(SiMe2)4Cl, (-OSiMe2SiMe2-)x; (inert atmosphere); addn. of CF3SO3H to the Sn compd. in toluene at -20°C, stirring (2 h), addn. of excess LiCl; filtration, solvent removal, NMR monitoring;
参考文献
Uhlig, Frank; Kayser, Christian; Klassen, Ralph; Hermann, Uwe; Brecker, Lothar; Schuermann, Markus; Ruhland-Senge, Karin; Englich, Ulrich
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1999 , vol. 54, # 2 p. 278 - 287