N,N,S-三甲基-S-苯基硫氮四氟硼酸盐合成路线 （共 22 条）
反应条件
sodium t-butanolate in tert-butyl alcohol
T=50°C; 48 h; Heating;
参考文献
Okuma, Kentaro; Nishimura, Kenshin; Ohta, Hiroshi
Chemistry Letters, 1984 , p. 93 - 96
反应条件
potassium tert-butylate in tert-butyl alcohol
144 h; Heating;
参考文献
Okuma, Kentaro; Nishimura, Kenshin; Ohta, Hiroshi
Chemistry Letters, 1984 , p. 93 - 96
反应条件
sodium t-butanolate in tert-butyl alcohol
T=50°C; 48 h; Heating;
参考文献
Okuma, Kentaro; Nishimura, Kenshin; Ohta, Hiroshi
Chemistry Letters, 1984 , p. 93 - 96
反应条件
sodium t-butanolate in tert-butyl alcohol
1.) 65 deg C, 2 h, 2.) reflux, 2 d;
参考文献
Okuma, Kentaro; Sato, Yasunari; Ishii, Toshiro; Ohta, Hiroshi
Journal of Organic Chemistry, 1994 , vol. 59, # 9 p. 2390 - 2392
反应条件
potassium tert-butylate in tert-butyl alcohol
24 h; Heating;
参考文献
Okuma, Kentaro; Nishimura, Kenshin; Ohta, Hiroshi
Chemistry Letters, 1984 , p. 93 - 96
反应条件
sodium t-butanolate in tert-butyl alcohol
48 h; Heating;
参考文献
Okuma, Kentaro; Nishimura, Kenshin; Ohta, Hiroshi
Chemistry Letters, 1984 , p. 93 - 96
反应条件
1,1-diphenyl-1,2-epoxyethane; sodium t-butanolate in tert-butyl alcohol
48 h; Heating;
参考文献
Okuma, Kentaro; Nishimura, Kenshin; Ohta, Hiroshi
Chemistry Letters, 1984 , p. 93 - 96
反应条件
1: N,N-(dimethylamino)-methylphenylsulfoxonium tetrafluoroborate With sodium hexamethyldisilazane in tetrahydrofuran
T=-78°C; 0.75 h; Inert atmosphere;
2: (formyl-2H)benzaldehyde in tetrahydrofuran
T=-78°C; 1.5 h; Inert atmosphere;
3: isobutyl phenyl ketene in tetrahydrofuran
T=-78 - 20°C; Inert atmosphere; diastereoselective reaction;
参考文献
Mondal, Mukulesh; Ho, Han-Jen; Peraino, Nicholas J.; Gary, Melanie A.; Wheeler, Kraig A.; Kerrigan, Nessan J.
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4587 - 4593
反应条件
1: N,N-(dimethylamino)-methylphenylsulfoxonium tetrafluoroborate With sodium hexamethyldisilazane in tetrahydrofuran
T=-78°C; 0.75 h; Inert atmosphere;
2: 18O-benzaldehyde in tetrahydrofuran
T=-78°C; 1.5 h; Inert atmosphere;
3: isobutyl phenyl ketene in tetrahydrofuran
T=-78 - 20°C; Inert atmosphere; diastereoselective reaction;
参考文献
Mondal, Mukulesh; Ho, Han-Jen; Peraino, Nicholas J.; Gary, Melanie A.; Wheeler, Kraig A.; Kerrigan, Nessan J.
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4587 - 4593
反应条件
potassium tert-butylate in tert-butyl alcohol
144 h; Heating;
参考文献
Okuma, Kentaro; Nishimura, Kenshin; Ohta, Hiroshi
Chemistry Letters, 1984 , p. 93 - 96
