1-(4-甲氧基苯基)-1,4-戊二酮合成路线 (共 31 条)
反应条件
2-(2-hydroxyethyl)-3-methyl-4-benzylthiazolium chloride; triethylamine
T=70°C; 12 h;
参考文献
Roth, B. D.; Ortwine, D. F.; Hoefle, M. L.; Stratton, C. D.; Sliskovic, D. R.; et al.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 1 p. 21 - 31
反应条件
tris(n-butyl)phosphine oxide in benzene
T=25°C; 1 h;
参考文献
Yasuda, Makoto; Oh-hata, Tatsuhiro; Shibata, Ikuya; Baba, Akio; Matsuda, Haruo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 7 p. 859 - 866
反应条件
in benzene
6 h; Irradiation;
参考文献
Matsumoto; Okubo; Mikami
Journal of the American Chemical Society, 1998 , vol. 120, # 16 p. 4015 - 4016
反应条件
1: DABCO / tetrahydrofuran / Ambient temperature
2: 41 percent / benzene / 6 h / Irradiation
View Scheme
参考文献
Matsumoto; Okubo; Mikami
Journal of the American Chemical Society, 1998 , vol. 120, # 16 p. 4015 - 4016
反应条件
hydrogenchloride; acetic acid
参考文献
Wilds; Johnson
Journal of the American Chemical Society, 1945 , vol. 67, p. 286,290
反应条件
1: AlCl3; carbon disulfide
2: benzene / auf Siedetemperatur
3: acetic acid; aqueous KOH
View Scheme
参考文献
Wilds; Johnson
Journal of the American Chemical Society, 1945 , vol. 67, p. 286,290
反应条件
1: benzene / auf Siedetemperatur
2: acetic acid; aqueous KOH
View Scheme
参考文献
Wilds; Johnson
Journal of the American Chemical Society, 1945 , vol. 67, p. 286,290
反应条件
tris(n-butyl)phosphine oxide
1 h; Ambient temperature;
参考文献
Baba, Akio; Yasuda, Makoto; Yano, Katsunori; Shibata, Ikuya; Matsuda, Haruo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 3205 - 3207
参考文献
Heck,R.F.
Journal of Organic Chemistry, 1965 , vol. 30, p. 2205 - 2208
反应条件
methanol; [RhCl(η2:η2-cycloocta-1,5-diene)]2; triphenylphosphine
T=80°C; P=15001.5 Torr; 18 h; AutoclaveInert atmosphere;
参考文献
Sauthier, Mathieu; Lamotte, Nicolas; Dheur, Julien; Castanet, Yves; Mortreux, Andre
New Journal of Chemistry, 2009 , vol. 33, # 5 p. 969 - 971