1-(4-甲氧基苯基)-1,4-戊二酮合成路线 （共 31 条）
反应条件
in dichloromethane
Irradiation;
参考文献
Coveney, Donal J.; Patel, Vinod F.; Pattenden, Gerald
Tetrahedron Letters, 1987 , vol. 28, # 47 p. 5949 - 5952
反应条件
hydrogenchloride; tin(ll) chloride in 1,4-dioxane
参考文献
Severin; Adam
Chemische Berichte, 1975 , vol. 108, # 1 p. 88 - 94
反应条件
lt;(CF3SO3Cu)2PhHgt;; calcium carbonate in benzene
0.05 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kozikowski, Alan P.; Ames, Anthony
Tetrahedron, 1985 , vol. 41, # 21 p. 4821 - 4834
反应条件
1: 95 percent / 2N HCl / diethyl ether / 0 °C
2: 88 percent / NaI, 12N HCl / acetone / 0.08 h / 0 °C
View Scheme
参考文献
Mayring, Lothar; Severin, Theodor
Chemische Berichte, 1981 , vol. 114, p. 3863 - 3877
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
24 h; Reflux;
参考文献
O'Reilly, Elaine; Iglesias, Cesar; Ghislieri, Diego; Hopwood, Jennifer; Galman, James L.; Lloyd, Richard C.; Turner, Nicholas J.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 9 p. 2447 - 2450
Angew. Chem., 2014 , vol. 53, # 9 p. 2479 - 2482,4
反应条件
1: aq. NaOH
2: (i) Ac2O, (ii) /BRN= 506021/, Et3N, CH2Cl2, (iii) aq. NaOH
View Scheme
参考文献
Nimgirawath,S. et al.
Australian Journal of Chemistry, 1976 , vol. 29, p. 339 - 356
反应条件
1: thionyl chloride
2: AlCl3
View Scheme
参考文献
Helberger
Justus Liebigs Annalen der Chemie, 1936 , vol. 522, p. 269,276
反应条件
aluminium trichloride
参考文献
Helberger
Justus Liebigs Annalen der Chemie, 1936 , vol. 522, p. 269,276
反应条件
(i) Ac2O, (ii) /BRN= 506021/, Et3N, CH2Cl2, (iii) aq. NaOH; Multistep reaction;
参考文献
Nimgirawath,S. et al.
Australian Journal of Chemistry, 1976 , vol. 29, p. 339 - 356
反应条件
(i) KOEt, (ii) aq. HCl, ascorbic acid, Cu; Multistep reaction;
参考文献
Severin; Koenig
Chemische Berichte, 1974 , vol. 107, # 5 p. 1499 - 1508
