2,4,6-三碘-3-甲基苯酚合成路线 (共 6 条)
反应条件
BnPh3P(+)(ICl2)(-); sodium hydrogencarbonate in methanol; dichloromethane T=20°C; 3.33333 h;
参考文献
Imanieh, Hossein; Ghammamy, Shahriar; Nikje, Mir Mohammad Alavi; Hosseini, Farhang; Aghbolagh, Zahra Shokri; Fun, Hoong-Kun; Khavasi, Hamid Reza; Kia, Reza
Helvetica Chimica Acta, 2011 , vol. 94, # 12 p. 2248 - 2255
反应条件
[K*18-crown-6]ICl2; potassium carbonate in acetonitrile T=25°C; 4 h; regioselective reaction;
参考文献
Mbatia, Hannah W.; Ulloa, Olbelina A.; Kennedy, Daniel P.; Incarvito, Christopher D.; Burdette, Shawn C.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 8 p. 2987 - 2991
反应条件
iodine; thallous acetate in dichloromethane 48 h; Ambient temperature;
参考文献
Gambie, Richard C.; Larsen, David S.; Rutledge, Peter S.; Woodgate, Paul D.
Australian Journal of Chemistry, 1997 , vol. 50, # 7 p. 767 - 769
反应条件
iodine in aq. buffer pH=Ca. 9;
参考文献
Gruzdeva; Kuzivanovb; Zenkevichc; Kondratenok
Russian Journal of Applied Chemistry, 2012 , vol. 85, # 9 p. 1355 - 1365
Russ. J. Appl. Chem, 2012 , vol. 85, # 9 p. 1355 - 1365,11
参考文献
Burger et al.
Journal of the American Chemical Society, 1945 , vol. 67, p. 1416,1417
参考文献
Kalle and Co.
Patent: DE106504 ;