1-(1H-吲哚-2-基)甲胺合成路线 (共 14 条)
反应条件
tetrahydrofuran; lithium aluminium tetrahydride
参考文献
Monatshefte fuer Chemie, , vol. 88, p. 1087,1093
反应条件
sodium n-propanolate in ethylene glycol dimethyl ether T=69.84°C; 6 h;
参考文献
Chen, Xinzhi; Zhou, Shaodong; Chen, Yuehan; Dong, Zehan; Gao, Yeyu; Qian, Chao; He, Chaohong
Research on Chemical Intermediates, 2012 , vol. 38, # 9 p. 2255 - 2269
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
反应条件
sodium tetrahydroborate; nickel dichloride in methanol T=20°C; 0.0833333 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 4 p. 691 - 701
反应条件
1: 99 percent / NH2OH*HCl; aq. Na2CO3 / ethanol / 0.5 h / Heating 2: NaBH4; NiCl2*6H2O / methanol / 0.08 h / 20 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 4 p. 691 - 701
反应条件
1: ammonia / CH2Cl2 / 10 h / 20 °C 2: lithium aluminum hydride / tetrahydrofuran / 7 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 63, # 23 p. 4983 - 4989
反应条件
1: 88 percent / ammonia / tetrahydrofuran; methanol / 840000 h / 20 °C 2: lithium aluminum hydride / tetrahydrofuran / 7 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 63, # 23 p. 4983 - 4989
反应条件
1: 83 percent / thionyl chloride / 3 h / Heating 2: 88 percent / ammonia / tetrahydrofuran; methanol / 840000 h / 20 °C 3: lithium aluminum hydride / tetrahydrofuran / 7 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 63, # 23 p. 4983 - 4989
反应条件
1: hydroxylamine hydrochloride; sodium carbonate / ethanol; water 2: sodium tetrahydroborate; NiII chloride hexahydrate / methanol View Scheme
参考文献
Journal of Agricultural and Food Chemistry, , vol. 60, # 32 p. 7792 - 7798
反应条件
methanol; sodium carbonate Yield given;
参考文献
Tetrahedron Letters, , vol. 31, # 48 p. 7011 - 7014