乙基alpha-乙酰氨基-alpha-乙氧羰基-beta-(7-氮杂-3-吲哚基)丙酸酯合成路线 （共 5 条）
参考文献
Journal of the American Chemical Society, , vol. 77, p. 457,458, 6554, 6555
参考文献
Robison; Robison
Journal of the American Chemical Society, 1955 , vol. 77, p. 457,458, 6554, 6555
反应条件
1: 1.) 2N NaOH, 2.) conc. HCl / 1.) dioxane, 40 deg C, 1 day, 2.) dioxane, reflux, 15 h
3: 40 percent / 6N HCl / 4 h / Heating
View Scheme
参考文献
Lecointe; Rolland-Fulcrand; Roumestant; Viallefont; Martinez
Tetrahedron Asymmetry, 1998 , vol. 9, # 10 p. 1753 - 1758
反应条件
1: 1.) 2N NaOH, 2.) conc. HCl / 1.) dioxane, 40 deg C, 1 day, 2.) dioxane, reflux, 15 h
2: 45 percent / phosphate buffer, CoCl2, Aspergillus genus acylase, 6N NaOH / 36 h / 40 °C
View Scheme
参考文献
Lecointe; Rolland-Fulcrand; Roumestant; Viallefont; Martinez
Tetrahedron Asymmetry, 1998 , vol. 9, # 10 p. 1753 - 1758
反应条件
hydrogenchloride; sodium hydroxide
1.) dioxane, 40 deg C, 1 day, 2.) dioxane, reflux, 15 h; Yield given. Multistep reaction;
参考文献
Lecointe; Rolland-Fulcrand; Roumestant; Viallefont; Martinez
Tetrahedron Asymmetry, 1998 , vol. 9, # 10 p. 1753 - 1758
