2-甲基-2-丙基[1-(4-氟苯基)-1-氧代-2-丙基]氨基甲酸酯合成路线 (共 3 条)
反应条件
triethylamine in N,N-dimethyl-formamide Acylation;
参考文献
Ermert; Hamacher; Coenen
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 14 p. 1345 - 1363
反应条件
1: bromine / CCl4 / 2 h 2: sodium azide / acetonitrile / 3 h / 60 °C 3: triethyl phosphite; hydrogen chloride / toluene / 0 - 20 °C 4: 76 percent / triethylamine / dimethylformamide View Scheme
参考文献
Ermert; Hamacher; Coenen
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 14 p. 1345 - 1363
反应条件
1: sodium azide / acetonitrile / 3 h / 60 °C 2: triethyl phosphite; hydrogen chloride / toluene / 0 - 20 °C 3: 76 percent / triethylamine / dimethylformamide View Scheme
参考文献
Ermert; Hamacher; Coenen
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 14 p. 1345 - 1363