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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
211245-67-9
合成路线
（共 7 条）
113548-13-3
+
211245-66-8
→
反应条件
211245-67-9
反应条件
in chloroform; ethyl acetate
参考文献
Booth, Richard John; Chatterjee, Arindam; Malone, Thomas Charles
Patent: US2004/224958 A1, 2004 ;
US 20040224958 A1
211245-66-8
→
反应条件
211245-67-9
反应条件
2-benzenesulfonyl-3-phenyl-oxaziridine in chloroform T=20°C;
参考文献
Barvian; Boschelli; Cossrow; Dobrusin; Fattaey; Fritsch; Fry; Harvey; Keller; Garrett; La; Leopold; McNamara; Quin; Trumpp-Kallmeyer; Toogood; Wu; Zhang
Journal of Medicinal Chemistry, 2000 , vol. 43, # 24 p. 4606 - 4616
770-31-0
4-氨基-2-甲巯基嘧啶-5-甲醛
→
反应条件
211245-67-9
反应条件
1.1: 75 percent / tetrahydrofuran / 3 h / Heating 2.1: 45 percent / N,N-diisopropylamine; 1,8-diazabicyclo[5.4.0]undec-7-ene / Heating 3.1: NaH / dimethylformamide / 50 °C 3.2: dimethylformamide / 50 °C 4.1: (+/-)-trans-2-(phenylsulfonyl)-3-phenyloxaziridine / CHCl3 / 20 °C View Scheme
参考文献
Barvian; Boschelli; Cossrow; Dobrusin; Fattaey; Fritsch; Fry; Harvey; Keller; Garrett; La; Leopold; McNamara; Quin; Trumpp-Kallmeyer; Toogood; Wu; Zhang
Journal of Medicinal Chemistry, 2000 , vol. 43, # 24 p. 4606 - 4616
588-36-3
2-甲硫基-4-氨基嘧啶-5-甲醇
→
反应条件
211245-67-9
反应条件
1.1: 100 percent / MnO2 / CHCl3 / 20 °C 2.1: 75 percent / tetrahydrofuran / 3 h / Heating 3.1: 45 percent / N,N-diisopropylamine; 1,8-diazabicyclo[5.4.0]undec-7-ene / Heating 4.1: NaH / dimethylformamide / 50 °C 4.2: dimethylformamide / 50 °C 5.1: (+/-)-trans-2-(phenylsulfonyl)-3-phenyloxaziridine / CHCl3 / 20 °C View Scheme
参考文献
Barvian; Boschelli; Cossrow; Dobrusin; Fattaey; Fritsch; Fry; Harvey; Keller; Garrett; La; Leopold; McNamara; Quin; Trumpp-Kallmeyer; Toogood; Wu; Zhang
Journal of Medicinal Chemistry, 2000 , vol. 43, # 24 p. 4606 - 4616
5909-24-0
4-氯-2-甲硫基嘧啶-5-羧酸乙酯
→
反应条件
211245-67-9
反应条件
1.1: 79 percent / Et3N; aq. NH4OH / tetrahydrofuran / 2.5 h / 20 °C 2.1: 76 percent / LiAlH4 / tetrahydrofuran / 0.5 h / 20 °C 3.1: 100 percent / MnO2 / CHCl3 / 20 °C 4.1: 75 percent / tetrahydrofuran / 3 h / Heating 5.1: 45 percent / N,N-diisopropylamine; 1,8-diazabicyclo[5.4.0]undec-7-ene / Heating 6.1: NaH / dimethylformamide / 50 °C 6.2: dimethylformamide / 50 °C 7.1: (+/-)-trans-2-(phenylsulfonyl)-3-phenyloxaziridine / CHCl3 / 20 °C View Scheme
参考文献
Barvian; Boschelli; Cossrow; Dobrusin; Fattaey; Fritsch; Fry; Harvey; Keller; Garrett; La; Leopold; McNamara; Quin; Trumpp-Kallmeyer; Toogood; Wu; Zhang
Journal of Medicinal Chemistry, 2000 , vol. 43, # 24 p. 4606 - 4616
776-53-4
2-甲硫基-4-氨基嘧啶-5-羧酸乙酯
→
反应条件
211245-67-9
反应条件
1.1: 76 percent / LiAlH4 / tetrahydrofuran / 0.5 h / 20 °C 2.1: 100 percent / MnO2 / CHCl3 / 20 °C 3.1: 75 percent / tetrahydrofuran / 3 h / Heating 4.1: 45 percent / N,N-diisopropylamine; 1,8-diazabicyclo[5.4.0]undec-7-ene / Heating 5.1: NaH / dimethylformamide / 50 °C 5.2: dimethylformamide / 50 °C 6.1: (+/-)-trans-2-(phenylsulfonyl)-3-phenyloxaziridine / CHCl3 / 20 °C View Scheme
参考文献
Barvian; Boschelli; Cossrow; Dobrusin; Fattaey; Fritsch; Fry; Harvey; Keller; Garrett; La; Leopold; McNamara; Quin; Trumpp-Kallmeyer; Toogood; Wu; Zhang
Journal of Medicinal Chemistry, 2000 , vol. 43, # 24 p. 4606 - 4616
211244-81-4
2-(甲基硫代)吡啶并[2,3-d]嘧啶-7(8h)-酮
→
反应条件
211245-67-9
反应条件
1.1: NaH / dimethylformamide / 50 °C 1.2: dimethylformamide / 50 °C 2.1: (+/-)-trans-2-(phenylsulfonyl)-3-phenyloxaziridine / CHCl3 / 20 °C View Scheme
参考文献
Barvian; Boschelli; Cossrow; Dobrusin; Fattaey; Fritsch; Fry; Harvey; Keller; Garrett; La; Leopold; McNamara; Quin; Trumpp-Kallmeyer; Toogood; Wu; Zhang
Journal of Medicinal Chemistry, 2000 , vol. 43, # 24 p. 4606 - 4616
