N-(3-苯基苯基)乙酰胺合成路线 （共 19 条）
反应条件
1: sodium acetate; glacial acetic acid; bromine 2: alcoholic hydrobromic acid / Hydrolysis.nachfolgend Eliminierung der Aminogruppe View Scheme
参考文献
Blakey; Scarborough
Journal of the Chemical Society, 1927 , p. 3006
反应条件
bis(1,5-cyclooctadiene)nickel (0); hydrogen; trimethylaluminum; tri-cyclo-hexyl-phosphine in toluene
T=130°C; P=750.075 Torr; 24 h; Schlenk technique;
参考文献
Patra, Tuhin; Agasti, Soumitra; Modak, Atanu; Maiti, Debabrata
Chemical Communications, 2013 , vol. 49, # 75 p. 8362 - 8364
反应条件
toluene-4-sulfonic acid in acetonitrile
T=70 - 80°C;
参考文献
Tamura, Yasumitsu; Yoshimoto, Yoshihiko; Sakai, Kiyoshi; Kita, Yasuyuki
Synthesis, 1980 , # 6 p. 483 - 484
反应条件
toluene-4-sulfonic acid in acetonitrile
T=70 - 80°C;
参考文献
Tamura, Yasumitsu; Yoshimoto, Yoshihiko; Sakai, Kiyoshi; Kita, Yasuyuki
Synthesis, 1980 , # 6 p. 483 - 484
反应条件
toluene-4-sulfonic acid in acetonitrile
T=70 - 80°C;
参考文献
Tamura, Yasumitsu; Yoshimoto, Yoshihiko; Sakai, Kiyoshi; Kita, Yasuyuki
Synthesis, 1980 , # 6 p. 483 - 484
反应条件
potassium phosphate; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in toluene
T=110°C; Suzuki-Miyaura Coupling; 24 h; Schlenk technique;
参考文献
Li, Xiao-Jian; Zhang, Jin-Ling; Geng, Yu; Jin, Zhong
Journal of Organic Chemistry, 2013 , vol. 78, # 10 p. 5078 - 5084
反应条件
palladium diacetate; cesium fluoride; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tert-butyl alcohol
T=110°C; Stille coupling; 14 h; Inert atmosphere;
参考文献
Naber, John R.; Fors, Brett P.; Wu, Xiaoxing; Gunn, Jonathon T.; Buchwald, Stephen L.
Heterocycles, 2010 , vol. 80, # 2 p. 1215 - 1226
参考文献
Fichter; Sulzberger
Chemische Berichte, 1904 , vol. 37, p. 882
反应条件
copper(II) bis(trifluoromethanesulfonate) in 1,2-dichloro-ethane
T=70°C; regioselective reaction;
参考文献
Phipps, Robert J.; Gaunt, Matthew J.
Science, 2009 , vol. 323, # 5921 p. 1593 - 1597
反应条件
1: phenyl trimethoxy silane; 3-chloro-aniline With 3-benzyl-1-(2-hydroxy-2-phenylethyl)imidazolium chloride; tetrabutylammomium bromide; water; palladium diacetate; sodium hydroxide
T=120°C; Hiyama coupling; 1 h; Microwave irradiation;
2: acetic anhydride
参考文献
Penafiel, Itziar; Pastor, Isidro M.; Yus, Miguel; Esteruelas, Miguel A.; Olivan, Montserrat; Onate, Enrique
European Journal of Organic Chemistry, 2011 , # 35 p. 7174 - 7181
