3-(2-吡啶基)-5,6-二苯基-1,2,4-三嗪合成路线 （共 16 条）
反应条件
tetrahydrofuran; oxygen; nitrogen(II) oxide
4 h; Ambient temperature;
参考文献
Itoh, Takashi; Matsuya, Yuji; Nagata, Kazuhiro; Ohsawa, Akio
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 9 p. 1547 - 1549
反应条件
tetraphosphorus decasulfide
T=210 - 215°C;
参考文献
Gianturco
Gazzetta Chimica Italiana, 1952 , vol. 82, p. 595,599
反应条件
1: diethyl ether / Ambient temperature
2: 1.) NaBH4, K3Fe(CN)6
View Scheme
参考文献
Konno, Shoetsu; Sagi, Mataichi; Yoshida, Nobuko; Yamanaka, Hiroshi
Heterocycles, 1987 , vol. 26, # 12 p. 3111 - 3114
反应条件
1: tBuONa / benzene / 20 °C
2: N2H4*H2O / ethanol / 3 h / Heating
View Scheme
参考文献
Nongkhlaw, Rishan Lang; Myrboh, Bekington
Heterocyclic Communications, 2006 , vol. 12, # 1 p. 67 - 72
反应条件
1: 56 percent / ethanol / 3 h / Heating
2: 22 percent / acetic anhydride / 1 h
View Scheme
参考文献
Gnichtel, Horst; Toepper, Bernhard
Liebigs Annalen der Chemie, 1989 , p. 1071 - 1074
反应条件
sodium acetate; copper(II) sulfate; acetic acid
参考文献
Laakso et al.
Tetrahedron, 1957 , vol. 1, p. 103,109
反应条件
acetic anhydride
1 h;
参考文献
Gnichtel, Horst; Toepper, Bernhard
Liebigs Annalen der Chemie, 1989 , p. 1071 - 1074
反应条件
hydrogenchloride; sodium nitrite
1) CHCl3, 0 deg C, 1.5 h, 2) r.t., 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Gonsalves, Antonio M. d'A. Rocha; Melo, Teresa M. V. D. Pinho e
Tetrahedron, 1992 , vol. 48, # 33 p. 6821 - 6826
反应条件
1: N2H4+H2O
2: CuSO4; sodium acetate; aqueous acetic acid
View Scheme
参考文献
Laakso et al.
Tetrahedron, 1957 , vol. 1, p. 103,109
参考文献
Gianturco
Gazzetta Chimica Italiana, 1952 , vol. 82, p. 595,599
