4-氨基-3-甲氧基苯甲酰胺合成路线 （共 3 条）
反应条件
hydrogen; palladium 10 on activated carbon in ethanol T=20°C; 19 h;
参考文献
DEVELOGEN AKTIENGESELLSCHAFT
Patent: WO2007/59905 A2, 2007 ;
Location in patent: Page/Page column 43 ;
WO 2007/059905 A2
反应条件
1.1: thionyl chloride; sodium hydroxide / 0.5 h / 80 °C 1.2: 0.5 h / 0 °C 2.1: sodium tetrahydroborate; methanol; NiII chloride hexahydrate / 0 - 23 °C View Scheme
参考文献
WANG, Aihua; Zhang, Yan; Leonard, Kristi Anne; Hawkins, Michael; Tounge, Brett Andrew; Maharoof, Umar S.M.; Barbay, Joseph Kent
Patent: US2012/129811 A1, 2012 ;
反应条件
1: ammonium hydroxide / water; tetrahydrofuran / 0.5 h / 0 °C 2: sodium tetrahydroborate; NiII chloride hexahydrate / methanol / 0.5 h / 0 - 23 °C View Scheme
参考文献
WANG, Aihua; Zhang, Yan; Leonard, Kristi Anne; Hawkins, Michael; Tounge, Brett Andrew; Maharoof, Umar S.M.; Barbay, Joseph Kent
Patent: US2012/129811 A1, 2012 ;
