Alpha,4-二氯茴香醚合成路线 (共 23 条)
反应条件
tert-butylhypochlorite; Ag(Phen)2OTf in acetonitrile T=20°C; 3 h; Inert atmosphere;
参考文献
Wang, Zhentao; Zhu, Lin; Yin, Feng; Su, Zhongquan; Li, Zhaodong; Li, Chaozhong
Journal of the American Chemical Society, 2012 , vol. 134, # 9 p. 4258 - 4263
反应条件
sulfuryl dichloride in dichloromethane 0.166667 h;
参考文献
Benneche, Tore; Undheim, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 2 p. 93 - 96
反应条件
Wilkinson's catalyst T=170°C; 0.5 h;
参考文献
Benneche, Tore; Undheim, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 6 p. 409 - 410
反应条件
phosphorus pentachloride; chlorine T=200°C;
参考文献
Journal of Applied Chemistry, , vol. 3, p. 409,411
US2733271 , ;
参考文献
Journal of Applied Chemistry, , vol. 3, p. 266,273
Journal of Applied Chemistry, , vol. 4, p. 110,111
反应条件
1: sodium hydroxide / 220 °C 2: thionyl chloride View Scheme
参考文献
Journal of Applied Chemistry, , vol. 3, p. 266,273
Journal of Applied Chemistry, , vol. 4, p. 110,111
反应条件
tetrachloromethane T=25°C; Irradiationvariation of temperature, and solvents; decarboxylation and H-atom abstraction rate constants of the benzoyloxyl radical, E(act.) and logA are given; KineticsThermodynamic dataMechanism;
参考文献
Chemistry Letters, , p. 357 - 360
反应条件
14.7 h; Ambient temperatureIrradiation; Quantum yieldMechanism;
参考文献
Journal of the American Chemical Society, , vol. 111, # 12 p. 4402 - 4407
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in toluene 1 h; Ambient temperature;
参考文献
Loubinoux, Bernard; Colin, Jean-Luc; Antonot-Colin, Brigitte; Lalloz, Lucien
Tetrahedron, 1987 , vol. 43, # 1 p. 93 - 100
反应条件
2,4-dichlorobenzeneacetonitrile; sodium hydride in N,N-dimethyl-formamide; benzene
参考文献
Heeres; Backx; Van Cutsem
Journal of Medicinal Chemistry, 1977 , vol. 20, # 11 p. 1516 - 1520