2-(2-苯基乙基)吡啶合成路线 （共 33 条）
反应条件
1: 70 percent / cuprous iodide, bis(triphenylphosphinyl)palladium dichloride / triethylamine / 1.) 0 deg C, 1 h, 2.) RT, 1 h
2: 93 percent / H2, Et3N / 10percent Pd/C / ethanol
View Scheme
参考文献
Tilley, Jefferson W.; Zawoiski, Sonja
Journal of Organic Chemistry, 1988 , vol. 53, # 2 p. 386 - 390
反应条件
1: 70 percent / cuprous iodide, bis(triphenylphosphinyl)palladium dichloride / triethylamine / 1.) 0 deg C, 1 h, 2.) RT, 1 h
2: 93 percent / H2, Et3N / 10percent Pd/C / ethanol
View Scheme
参考文献
Tilley, Jefferson W.; Zawoiski, Sonja
Journal of Organic Chemistry, 1988 , vol. 53, # 2 p. 386 - 390
反应条件
Dimethylammonium sulphite
T=190 - 200°C; 14 h; Yields of byproduct given;
参考文献
Kost, A. N.; Yudin, L. G.; Rumyantsev, A. N.; Sagitullin, R. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 2 p. 215
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , # 2 p. 270
反应条件
ethylammonium sulphite
T=190 - 200°C; Yields of byproduct given;
参考文献
Kost, A. N.; Yudin, L. G.; Rumyantsev, A. N.; Sagitullin, R. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 2 p. 215
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , # 2 p. 270
反应条件
n-butylammonium sulfite
T=190 - 200°C; Yields of byproduct given;
参考文献
Kost, A. N.; Yudin, L. G.; Rumyantsev, A. N.; Sagitullin, R. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 2 p. 215
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , # 2 p. 270
反应条件
sodium hydroxide; hydrazine hydrate; diethylene glycol
参考文献
Zelinski; Benilda
Journal of the American Chemical Society, 1951 , vol. 73, p. 696
反应条件
1: diethyl ether / bei Siedetemperatur
2: hydrazine hydrate; sodium hydroxide; diethylene glycol
View Scheme
参考文献
Zelinski; Benilda
Journal of the American Chemical Society, 1951 , vol. 73, p. 696
反应条件
1: diethyl ether / bei Siedetemperatur
2: hydrazine hydrate; sodium hydroxide; diethylene glycol
View Scheme
参考文献
Zelinski; Benilda
Journal of the American Chemical Society, 1951 , vol. 73, p. 696
反应条件
triphenyl phosphite; methanol; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2
参考文献
Ogiwara, Yohei; Kochi, Takuya; Kakiuchi, Fumitoshi
Organic Letters, 2011 , vol. 13, # 12 p. 3254 - 3257
反应条件
1.1: 61 percent / NaH; 15-crown-5 / tetrahydrofuran
2.1: Na / tetrahydrofuran / 12 h / 0 °C
2.2: 78 percent / H2O / tetrahydrofuran / cooling
View Scheme
参考文献
Azzena, Ugo; Dettori, Giovanna; Lubinu, Caterina; Mannu, Alberto; Pisano, Luisa
Tetrahedron, 2005 , vol. 61, # 36 p. 8663 - 8668
