反应条件
1: 1.) n-BuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 1 h; 2.) rt, 6 h
2: LiBr / acetone / 12 h / 25 °C
3: 25 percent Chromat. / Cl2ZrCp2 / CH2Cl2 / 6 h / 25 °C
View Scheme
参考文献
Negishi,E.; Boardman,L.D.; Sawada,H.
Journal of the American Chemical Society, 1988 , vol. 110, p. 5383
