in toluene
soln. of Me2Si(tBuN)2Sn added dropwise to a soln. of the silylamine in toluene, stirring for two hours, refluxing for one hour, volatile substances removed in vacuum and the seconocubane-like intermediate pyrolysed in vacuo at 0.01 Torr and 250°C; product sublimed, elem. anal.;
参考文献
Veith, Michael; Opsoelder, Michael; Zimmer, Michael; Huch, Volker
European Journal of Inorganic Chemistry, 2000 , # 6 p. 1143 - 1146
Sheludyakov,V.D. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1976 , vol. 46, # 12 p. 2712 - 2719,2589 - 2594
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Sommer,P.; Birkofer,L.
Journal of Organometallic Chemistry, 1975 , vol. 99, p. C1 - C4
