反应条件
in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
(Ar); soln. of SmI2 (2 equiv.) in THF was added to soln. of Bu3GeCl and Me3GeBr (1/1) in hexamethylphosphoric triamide; mixt. was stirred at room temp. for 15 h; chromd. (silica gel, ether); evapd.; chromd. (silica gel, hexane);
参考文献
Azemi, Takushi; Yokoyama, Yasuo; Mochida, Kunio
Journal of Organometallic Chemistry, 2005 , vol. 690, # 6 p. 1588 - 1593
