顺-1,5-二甲基二环(3.3.0)辛烷-3,7-二酮合成路线 (共 5 条)
反应条件
in water; acetic acid 7 h; Heating;
参考文献
Coates, Robert M.; Shach, Shrenik K.; Mason, Robert W.
Journal of the American Chemical Society, 1982 , vol. 104, # 8 p. 2198 - 2208
反应条件
2: POCl3, pyridine
View Scheme
参考文献
Quast, Helmut; Goerlach, Yvonne; Meichsner, Georg; Peters, Karl; Peters, Eva-Maria; Schnering, Hans Georg von
Tetrahedron Letters, 1982 , vol. 23, # 45 p. 4677 - 4680
反应条件
Title compound not separated from byproducts;
参考文献
Camps, P.; Iglesias, C.; Lozano, R.; Miranda, M. A.; Rodriguez, M. J.
Tetrahedron Letters, 1987 , vol. 28, # 16 p. 1831 - 1832
反应条件
Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Quast, Helmut; Mayer, Andreas
Liebigs Annalen der Chemie, 1988 , p. 1155 - 1164
反应条件
sodium hydride in dimethyl sulfoxide
T=60°C; 88 h;
参考文献
Gleiter, Rolf; Jaehne, Gerhard; Mueller, Georg; Nixdorf, Matthias; Irngartinger, Hermann
Helvetica Chimica Acta, 1986 , vol. 69, p. 71 - 84