苯甲醇-Alpha,Alpha-d2合成路线 （共 34 条）
反应条件
thionyl chloride; magnesium
Multistep reaction;
参考文献
Gessner, Uwe; Heesing, Albert
Chemische Berichte, 1985 , vol. 118, # 7 p. 2593 - 2606
反应条件
1.1: pyridinium chlorochromate / dichloromethane / 20 °C
2.1: potassium tert-butylate / diethyl ether / 3 h / Inert atmosphere
2.2: 20 °C / Reflux; Inert atmosphere
View Scheme
参考文献
Meng, Ling-Guo; Wang, Lei
Chemical Communications, 2012 , vol. 48, # 26 p. 3242 - 3244
反应条件
1,4-diaza-bicyclo[2.2.2]octane; [RuCl2(IiPr)(p-cymene)] in toluene
30 h; Inert atmosphereMolecular sieveReflux;
参考文献
Maggi, Agnese; Madsen, Robert
Organometallics, 2012 , vol. 31, # 1 p. 451 - 455
反应条件
1: 91 percent / phosphorus tribromide
2: 87 percent / lithium aluminum hydride
3: 1.) p-toluenesulfochloride, 2.) fluoride
View Scheme
参考文献
Dneprovskii, A. S.; Eliseenkov, E. V.; Mil'tsov, S. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 317 - 324
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 2 p. 365 - 373
