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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
211814-64-1
合成路线
（共 8 条）
293299-52-2
→
反应条件
211814-64-1
反应条件
diethylzinc; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; Reduction; 1 h;
参考文献
Ohno, Hiroaki; Miyamura, Kumiko; Tanaka, Tetsuaki; Oishi, Shinya; Toda, Ayako; Takemoto, Yoshiji; Fujii, Nobutaka; Ibuka, Toshiro
Journal of Organic Chemistry, 2002 , vol. 67, # 4 p. 1359 - 1367
293299-45-3
→
反应条件
211814-64-1
反应条件
diethylzinc; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; Reduction; 1 h;
参考文献
Ohno, Hiroaki; Miyamura, Kumiko; Tanaka, Tetsuaki; Oishi, Shinya; Toda, Ayako; Takemoto, Yoshiji; Fujii, Nobutaka; Ibuka, Toshiro
Journal of Organic Chemistry, 2002 , vol. 67, # 4 p. 1359 - 1367
5558-11-2
+
98-59-9
对甲苯磺酰氯
→
反应条件
211814-64-1
反应条件
triethylamine in dichloromethane T=0 - 20°C;
参考文献
Ma, Shengming; Yu, Fei; Gao, Wenzhong
Journal of Organic Chemistry, 2003 , vol. 68, # 15 p. 5943 - 5949
13379-98-1
→
反应条件
211814-64-1
反应条件
1: (COCl)2; DMSO; diisopropylethylamine / CH2Cl2 / 1.33 h / -78 °C 2: 777 mg / CHCl3 / 19 h / 0 °C 3: 63 percent / DIBAL / CHCl3; toluene / 2 h / -78 °C 4: 99 percent / Et3N / tetrahydrofuran / 0.5 h / -78 - 0 °C 5: 66 percent / Et2Zn; Pd(PPh3)4 / tetrahydrofuran; toluene / 1 h / 20 °C View Scheme
参考文献
Ohno, Hiroaki; Miyamura, Kumiko; Tanaka, Tetsuaki; Oishi, Shinya; Toda, Ayako; Takemoto, Yoshiji; Fujii, Nobutaka; Ibuka, Toshiro
Journal of Organic Chemistry, 2002 , vol. 67, # 4 p. 1359 - 1367
98-59-9
对甲苯磺酰氯
→
反应条件
211814-64-1
反应条件
1: 99 percent / Et3N / CH2Cl2 / 17 h / 0 °C 2: (COCl)2; DMSO; diisopropylethylamine / CH2Cl2 / 1.33 h / -78 °C 3: 777 mg / CHCl3 / 19 h / 0 °C 4: 63 percent / DIBAL / CHCl3; toluene / 2 h / -78 °C 5: 99 percent / Et3N / tetrahydrofuran / 0.5 h / -78 - 0 °C 6: 66 percent / Et2Zn; Pd(PPh3)4 / tetrahydrofuran; toluene / 1 h / 20 °C View Scheme
参考文献
Ohno, Hiroaki; Miyamura, Kumiko; Tanaka, Tetsuaki; Oishi, Shinya; Toda, Ayako; Takemoto, Yoshiji; Fujii, Nobutaka; Ibuka, Toshiro
Journal of Organic Chemistry, 2002 , vol. 67, # 4 p. 1359 - 1367
718633-51-3
→
反应条件
211814-64-1
反应条件
1: 777 mg / CHCl3 / 19 h / 0 °C 2: 63 percent / DIBAL / CHCl3; toluene / 2 h / -78 °C 3: 99 percent / Et3N / tetrahydrofuran / 0.5 h / -78 - 0 °C 4: 66 percent / Et2Zn; Pd(PPh3)4 / tetrahydrofuran; toluene / 1 h / 20 °C View Scheme
参考文献
Ohno, Hiroaki; Miyamura, Kumiko; Tanaka, Tetsuaki; Oishi, Shinya; Toda, Ayako; Takemoto, Yoshiji; Fujii, Nobutaka; Ibuka, Toshiro
Journal of Organic Chemistry, 2002 , vol. 67, # 4 p. 1359 - 1367
405932-44-7
→
反应条件
211814-64-1
反应条件
1: 99 percent / Et3N / tetrahydrofuran / 0.5 h / -78 - 0 °C 2: 66 percent / Et2Zn; Pd(PPh3)4 / tetrahydrofuran; toluene / 1 h / 20 °C View Scheme
参考文献
Ohno, Hiroaki; Miyamura, Kumiko; Tanaka, Tetsuaki; Oishi, Shinya; Toda, Ayako; Takemoto, Yoshiji; Fujii, Nobutaka; Ibuka, Toshiro
Journal of Organic Chemistry, 2002 , vol. 67, # 4 p. 1359 - 1367
405932-38-9
→
反应条件
211814-64-1
反应条件
1: 95 percent / DIBAL-H / CHCl3; toluene / 2 h / -78 °C 2: 99 percent / Et3N / tetrahydrofuran / 2 h / -78 - 0 °C 3: 69 percent / Et2Zn; Pd(PPh3)4 / tetrahydrofuran; toluene / 0.5 h / 20 °C View Scheme
参考文献
Ohno, Hiroaki; Miyamura, Kumiko; Tanaka, Tetsuaki; Oishi, Shinya; Toda, Ayako; Takemoto, Yoshiji; Fujii, Nobutaka; Ibuka, Toshiro
Journal of Organic Chemistry, 2002 , vol. 67, # 4 p. 1359 - 1367
