反应条件
1.1: 0.17 h / Reflux
2.1: sodium hydroxide
2.2: 20 h / Reflux
3.1: thionyl chloride
4.1: pyridine; 4-(N,N-dimethlyamino)pyridine / diethyl ether / 0.33 h
5.1: 2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride / benzene / 25 °C / Cooling with liquid nitrogen; Sealed tube; UV-irradiation
View Scheme
参考文献
Beckwith, Athelstan L. J.; Schiesser, Carl H.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 6 p. 1736 - 1743
