2-氨甲基-2,3-二氢苯并呋喃合成路线 （共 6 条）
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=20°C; 4 h; Heating / reflux; 2: With water in tetrahydrofuran T=0°C;
参考文献
Gomtsyan, Arthur; Bayburt, Erol K.; Schmidt, Robert G.; Lee, Chih-Hung; Brown, Brian S.; Jinkerson, Tammie K.; Koenig, John R.; Daanen, Jerome F.; Latshaw, Steven P.
Patent: US2006/128689 A1, 2006 ;
Location in patent: Page/Page column 19 ;
反应条件
palladium 10 on activated carbon; hydrogen in ethanol T=20°C;
参考文献
Chen, Wen; Yang, Xiao-Dong; Li, Yan; Yang, Li-Juan; Wang, Xue-Quan; Zhang, Gao-Lan; Zhang, Hong-Bin
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 11 p. 4250 - 4255
反应条件
1: sodium azide; copper / N,N-dimethyl-formamide / 90 °C 2: palladium 10 on activated carbon; hydrogen / ethanol / 20 °C View Scheme
参考文献
Chen, Wen; Yang, Xiao-Dong; Li, Yan; Yang, Li-Juan; Wang, Xue-Quan; Zhang, Gao-Lan; Zhang, Hong-Bin
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 11 p. 4250 - 4255
反应条件
1: 210 °C / Microwave irradiation 2: iodine / ethanol; water / 12 h / 50 °C 3: sodium azide; copper / N,N-dimethyl-formamide / 90 °C 4: palladium 10 on activated carbon; hydrogen / ethanol / 20 °C View Scheme
参考文献
Chen, Wen; Yang, Xiao-Dong; Li, Yan; Yang, Li-Juan; Wang, Xue-Quan; Zhang, Gao-Lan; Zhang, Hong-Bin
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 11 p. 4250 - 4255
反应条件
1: iodine / ethanol; water / 12 h / 50 °C 2: sodium azide; copper / N,N-dimethyl-formamide / 90 °C 3: palladium 10 on activated carbon; hydrogen / ethanol / 20 °C View Scheme
参考文献
Chen, Wen; Yang, Xiao-Dong; Li, Yan; Yang, Li-Juan; Wang, Xue-Quan; Zhang, Gao-Lan; Zhang, Hong-Bin
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 11 p. 4250 - 4255
反应条件
1: potassium carbonate / acetone / Reflux 2: 210 °C / Microwave irradiation 3: iodine / ethanol; water / 12 h / 50 °C 4: sodium azide; copper / N,N-dimethyl-formamide / 90 °C 5: palladium 10 on activated carbon; hydrogen / ethanol / 20 °C View Scheme
参考文献
Chen, Wen; Yang, Xiao-Dong; Li, Yan; Yang, Li-Juan; Wang, Xue-Quan; Zhang, Gao-Lan; Zhang, Hong-Bin
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 11 p. 4250 - 4255
