(17beta)-17-乙炔基-3-羟基雌甾-1,3,5(10)-三烯-17-基乙酸酯合成路线 （共 4 条）
反应条件
potassium carbonate in methanol T=20°C; Deacetylation; 0.5 h;
参考文献
Werschkun, Barbara; Gorziza, Karin; Thiem, Joachim
Journal of Carbohydrate Chemistry, 1999 , vol. 18, # 6 p. 629 - 637
反应条件
1: 100 percent / pyridine / 48 h / 100 °C 2: 66 percent / potassium carbonate / methanol / 0.5 h / 20 °C View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 18, # 6 p. 629 - 637
反应条件
1: 61 percent / boron trifluoride diethyl etherate / CH2Cl2 / 0.5 h / -20 °C 2: 74 percent / sodium hydroxide / methanol / 48 h / 20 °C View Scheme
参考文献
Werschkun, Barbara; Gorziza, Karin; Thiem, Joachim
Journal of Carbohydrate Chemistry, 1999 , vol. 18, # 6 p. 629 - 637
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-20°C; glucuronidation; 0.5 h;
参考文献
Werschkun, Barbara; Gorziza, Karin; Thiem, Joachim
Journal of Carbohydrate Chemistry, 1999 , vol. 18, # 6 p. 629 - 637
