4,5-二苯基-1,3-二氧戊环烯-2-酮合成路线 (共 17 条)
参考文献
Wilson, R. Marshall; Chow, Tahsin J.
Tetrahedron Letters, 1983 , vol. 24, # 43 p. 4635 - 4636
参考文献
Wilson, R. Marshall; Chow, Tahsin J.
Tetrahedron Letters, 1983 , vol. 24, # 43 p. 4635 - 4636
反应条件
di(n-butyl)tin oxide
1.) toluene, reflux, 1 h, 2.) toluene, 0 deg C, 20 min ---> room temperature; Yield given. Multistep reaction;
参考文献
Davies, Alwyn G.; Hawari, Jalal A.-A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 875 - 882
反应条件
di(n-butyl)tin oxide
1.) toluene, reflux, 1 h; Yield given. Multistep reaction;
参考文献
Davies, Alwyn G.; Hawari, Jalal A.-A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 875 - 882
反应条件
di(n-butyl)tin oxide
1.) toluene, reflux, 1 h, 2.) toluene, 30 min; Yield given. Multistep reaction;
参考文献
Davies, Alwyn G.; Hawari, Jalal A.-A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 875 - 882
反应条件
trifluoroacetic acid
1) DMF, 0 deg C to room temperature, 30 min, 2) overnight; Yield given. Multistep reaction;
参考文献
Lotz, Bruce T.; Miller, Marvin J.
Journal of Organic Chemistry, 1993 , vol. 58, # 3 p. 618 - 625
反应条件
(i) <Me4N>OH, MeOH, (ii) /BRN= 1114120/, DMF, (iii) CF3CO2H; Multistep reaction;
参考文献
Sheehan,J.C.; Guziec,F.S.
Journal of Organic Chemistry, 1973 , vol. 38, p. 3034 - 3040